Characterization of Synthesized Titanium Oxide Nanoclusters by MALDI-TOF Mass Spectrometry

Journal of the American Society for Mass Spectrometry

Volumn 18, Issue 3, 2007, Pages 517-524

  Guan, Bing ^a   Lu, Weigang ^a   Fang, Jiye ^a   Cole, Richard B ^a  

^a UNIVERSITY OF NEW ORLEANS   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

MASS SPECTROMETRY; PARTICLE SIZE ANALYSIS; TITANIUM OXIDES; TRANSMISSION ELECTRON MICROSCOPY;

NANOPARTICLES; SIZE SELECTION TREATMENT; SYNTHESIZED TITANIUM OXIDE NANOCLUSTERS; THERMAL SOLVENT PROCESS;

NANOSTRUCTURED MATERIALS;

NANOMATERIAL; NANOPARTICLE; SOLVENT; TITANIUM DIOXIDE;

ARTICLE; CHEMICAL ANALYSIS; MATERIALS TESTING; MATRIX ASSISTED LASER DESORPTION IONIZATION TIME OF FLIGHT MASS SPECTROMETRY; NANOCHEMISTRY; NANOTECHNOLOGY; PARTICLE SIZE; TRANSMISSION ELECTRON MICROSCOPY;

MASS SPECTROMETRY; NANOPARTICLES; PARTICLE SIZE; SPECTROMETRY, MASS, MATRIX-ASSISTED LASER DESORPTION-IONIZATION; TITANIUM;

EID: 33847078730     PISSN: 10440305     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jasms.2006.10.021     Document Type: Article

References (55)

1. Fujishima A., Rao T.N., and Tryk D.A. Photocatalysts and Diamond Electrodes. Electrochim. Acta 45 (2000) 4683-4690
2. Hoffmann M.R., Martin S.T., Choi W.Y., and Bahnemann D.W. Environmental Applications of Semiconductor Photocatalysis. Chem. Rev. 95 (1995) 69-96
3. 2 Surfaces-Principles, Mechanisms, and Selected Results. Chem. Rev. 95 (1995) 735-758
4. 2 Thin Films by a Novel Sol-Gel Processing for Gas Sensor Applications. Sens. Actuators B Chem. 68 (2000) 189-196
5. 2 Films. Thin Solid Films 176 (1989) 181-186
6. Venz P.A., Kloprogge J.T., and Frost R.L. Chemically Modified Titania Hydrolysates: Physical Properties. Langmuir 16 (2000) 4962-4968
7. 2 Films. Nature 353 (1991) 737-740
8. Hagfeldt A., and Gratzel M. Light-Induced Redox Reactions in Nanocrystalline Systems. Chem. Rev. 95 (1995) 49-68
9. Henrich V.E., and Cox P.A. The Surface Science of Metal Oxides (1994), Cambridge Univ. Press, New York
10. 2 (110) Surface. Surf. Sci. 50 (1996) 159-175
11. Sousa C., and Illas F. Ionic-Covalent Transition in Titanium-Oxides. Phys. Rev. B 50 (1994) 13974-13980
12. 2 (Rutile) Clusters. Int. J. Quantum Chem. 44 (1992) 477-495
13. 8. Inorg. Chem. 28 (1989) 4439-4445
14. Schubert U., Arpac E., Glaubitt W., Helmerich A., and Chau C. Primary Hydrolysis Products of Methacrylate-Modified Titanium and Zirconium Alkoxides. Chem. Mater. 4 (1992) 291-295
15. Wilcoxon J.P., Martin J.E., and Provencio P. Size Distributions of Gold Nanoclusters Studied by Liquid Chromatography. Langmuir 16 (2000) 9912-9920
16. Cullity B.D. Elements of X-ray Diffraction (1978), Addison-Wesley, Reading, MA
17. Kubler B., Millon E., Gaumet J.J., and Muller J.F. Formation of High mass C∼n Clusters (n > 100) by Laser Ablation/Desorption Coupled with Mass Spectrometry. Fullerene Sci. Technol. 4 (1996) 1247-1261
18. 2. Science 269 (1995) 1554-1556
19. Lafargue P.E., Gaumet J.J., Muller J.F., and Labrosse A. Laser Ablation of Silica: Study of Induced Clusters by Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. J. Mass Spectrom. 31 (1996) 623-632
20. Kasuya A., Sivamohan R., Barnakov Y.A., Dmitruk I.M., Nirasawa T., Romanyuk V.R., Kumar V., Mamykin S.V., Tohji K., Jeyadevan B., Shinoda K., Kudo T., Terasaki O., Liu Z., Belosludov R.V., Sundararajan V., and Kawazoe Y. Ultra-stable Nanoparticles of CdSe Revealed from Mass Spectrometry. Nat. Mater. 3 (2004) 99-102
21. Khitrov G.A., and Strouse G.F. ZnS Nanomaterial Characterization by MALDI-TOF Mass Spectrometry. J. Am. Chem. Soc. 125 (2003) 10465-10469
22. Gaumet J.J., and Strouse G.F. Nanospray Mass Spectrometry Technique for Analyzing Nanomaterials from Molecular Precursors up to 1.5 nm in Diameter Clusters. Mater. Sci. Eng. C 19 (2002) 299-304
23. 4]. Nano. Lett. 2 (2002) 375-379
24. Gaumet J.J., and Strouse G.F. Electrospray Mass Spectrometry of Semiconductor Nanoclusters: Comparative Analysis of Positive and Negative Ion Mode. J. Am. Soc. Mass Spectrom. 11 (2000) 338-344
25. Schaaff T.G., Shafigullin M.N., Khoury J.T., Vezmar I., and Whetten R.L. Properties of a Ubiquitous 29 kDa Au:SR Cluster Compound. J. Phys. Chem. B 105 (2001) 8785-8796
26. Whetten R.L., Khoury J.T., Alvarez M.M., Murthy S., Vezmar I., Wang Z.L., Stephens P.W., Cleveland C.L., Luedtke W.D., and Landman U. Nanocrystal Gold Molecules. Adv. Mater. 8 (1996) 428-433
27. Arnold R.J., and Reilly J.P. High-resolution Time-of-Flight Mass Spectra of Alkanethiolate-coated Gold Nanocrystals. J. Am. Chem. Soc. 120 (1998) 1528-1532
28. Vezmar I., Alvarez M.M., Khoury J.T., Salisbury B.E., Shafigullin M.N., and Whetten R.L.Z. Cluster Beams from Passivated Nanocrystals. Z. Phys. D: At. Mol. Clusters 40 (1997) 147-151
29. d'Avray A.T.D., Carpenter E.E., O'Connor C.J., and Cole R.B. Characterization of Ferrite Nanoparticles by Laser Desorption/Ionization Mass Spectrometry. Eur. Mass Spectrom. 4 (1998) 441-449
30. 8 by Electrospray Time of Flight Mass Spectrometry. J. Am. Soc. Mass Spectrom. 15 (2004) 260-267
31. Mori H., Lanzendorfer M.G., Muller A.H.E., and Klee J.E. Silsesquioxane-based Nanoparticles Formed via Hydrolytic Condensation of Organotriethoxysilane Containing Hydroxy Groups. Macromolecules 37 (2004) 5228-5238
32. Alves S., Kalberer M., and Zenobi R. Direct Detection of Particles Formed by Laser Ablation of Matrices during Matrix-assisted Laser Desorption/Ionization. Rapid Commun. Mass Spectrom. 17 (2003) 2034-2038
33. Bauer F., Sauerland V., Ernst H., Glasel H.A., Naumov S., and Mehnert R. Preparation of Scratch- and Abrasion-resistant Polymeric Nanocomposites by Monomer Grafting onto Nanoparticles, 4. Application of MALDI-TOF Mass Spectrometry to the Characterization of Surface Modified Nanoparticles. Macromol. Chem. Phys. 204 (2003) 375-383
34. Colton R., Dagostino A., and Traeger J.C. Electrospray Mass Spectrometry Applied Inorganic and Organometallic Chemistry. Mass Spectrom. Rev. 14 (1995) 79-106
35. Gatlin C.L., and Turecek F. In: Cole R.B. (Ed). Electrospray Ionization Mass Spectrometry: Fundamentals, Instrumentation, and Applications (1997), Wiley-Interscience, New York
36. Traeger J.C. Electrospray Mass Spectrometry of Organometallic Compounds. Int. J. Mass. Spectrom. 200 (2000) 387-401
37. Lover T., Henderson W., Bowmaker G.A., Seakins J.M., and Cooney R.P. Electrospray Mass Spectrometry of Thiophenolate-capped Clusters of CdS, CdSe, and ZnS and of Cadmium and Zinc Thiophenolate Complexes: Observation of Fragmentation and Metal, Chalcogenide, and Ligand Exchange Processes. Inorg. Chem. 36 (1997) 3711-3723
38. Lover T., Henderson W., Bowmaker G.A., Seakins J.M., and Cooney R.P. Functionalization and Capping of a CdS Nanocluster: A Study of Ligand Exchange by Electrospray Mass Spectrometry. Chem. Mater. 9 (1997) 1878-1886
39. Spengler B., Kirsch D., and Kaufmann R. Metastable Decay of Peptides and Proteins in Matrix-assisted Laser-Desorption Mass-Spectrometry. Rapid Commun. Mass Spectrom. 5 (1991) 198-202
40. Spengler B., Kirsch D., Kaufmann R., and Jaeger E. Peptide Sequencing by Matrix-Assisted Laser-Desorption Mass-Spectrometry. Rapid Commun. Mass Spectrom. 6 (1992) 105-108
41. 2 Polymorphs. J. Am. Ceram. Soc. 62 (1979) 356-357
42. Cheng H.M., Ma J.M., Zhao Z.G., and Qi L.M. Hydrothermal Preparation of Uniform Nanosize Rutile and Anatase Particles. Chem. Mater. 7 (1995) 663-671
43. International Centre for Diffraction Data (ICDD, formerly JCPDS), File no. 21-1272; ICDD: Newtown Square, PA.
44. Chen L.X., Rajh T., Jager W., Nedeljkovic J., and Thurnauer M.C. X-ray Absorption Reveals Surface Structure of Titanium Dioxide Nanoparticles. J. Synchrotron. Radiat. 6 (1999) 445-447
45. 2 Nanoparticles and Photocatalytic Reduction of Metal Ions. J. Phys. Chem. B 101 (1997) 10688-10697
46. 2 Nanoparticles. Chem. Phys. Lett. 344 (2001) 31-39
47. Naicker P.K., Cummings P.T., Zhang H.Z., and Banfield J.F. Characterization of Titanium Dioxide Nanoparticles Using Molecular Dynamics Simulations. J. Phys. Chem. B 109 (2005) 15243-15249
48. 2-Matrix-assisted Laser Desorption/Ionization Mass Spectrometry for Selectively Detecting alpha-Cyclodextrin. Anal. Chem. 76 (2004) 1453-1457
49. Chen C.T., and Chen Y.C. Desorption/Ionization Mass Spectrometry on Nanocrystalline Titania Sol-Gel-deposited Films. Rapid Commun. Mass Spectrom. 18 (2004) 1956-1964
50. Kinumi T., Saisu T., Takayama M., and Niwa H. Matrix-assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry Using an inorganic Particle Matrix for Small Molecule Analysis. J. Mass Spectrom. 35 (2000) 417-422
51. Dopke N.C., Treichel P.M., and Vestling M.M. Matrix-assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF MS) of Rhenium(III) Halides: A Characterization Tool for Metal Atom Clusters. Inorg. Chem. 37 (1998) 1272-1277
52. 4. Rapid Commun. Mass Spectrom. 17 (2003) 2649-2654
53. 4. Rapid Commun. Mass Spectrom. 14 (2000) 662-668
54. 4. Rapid Commun. Mass Spectrom. 15 (2001) 386-392
55. Schaaff T.G. Laser Desorption and Matrix-assisted Laser Desorption/Ionization Mass Spectrometry of 29-kDa Au:SR Cluster Compounds. Anal. Chem. 76 (2004) 6187-6196