Tetranuclear grid-like copper(II) complexes with pyrazolate bridges: Syntheses, structures, magnetic and EPR spectroscopic properties

Journal of the Chemical Society - Dalton Transactions

Volumn , Issue 3, 1999, Pages 339-348

  Mann, Karen L V ^a   Psillakis, Elefteria ^a   Jeffery, John C ^a   Rees, Leigh H ^a   Harden, Nicholas M ^a   McCleverty, Jon A ^a   Ward, Michael D ^a   Gatteschi, Dante ^b   Totti, Federico ^b   Mabbs, Frank E ^c   McInnes, Eric J L ^c   Riedi, Peter C ^d   Smith, Graham M ^d  

^a UNIVERSITY OF BRISTOL   (United Kingdom)

^b UNIVERSITY OF FLORENCE   (Italy)

^c UNIVERSITY OF MANCHESTER   (United Kingdom)

^d UNIVERSITY OF ST ANDREWS   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33847004805     PISSN: 03009246     EISSN: None     Source Type: Journal    
DOI: 10.1039/a807599i     Document Type: Article

References (46)

1. D. Philp and J. F. Stoddart, Angew. Chem., Int. Ed. Engl., 1996, 35, 1155;
2. J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995;
3. C. Piguet, G. Bernardinelli and G. Hopfgartner, Chem. Rev., 1997, 97, 2005.
4. T. Beissel, R. E. Powers and K. N. Raymond, Angew. Chem., Int. Ed. Engl., 1996, 35, 1084.
5. A. J. Amoroso, A. M. W. Cargill Thompson, J. P. Maher, J. A. McCleverty and M. D. Ward, Inorg. Chem., 1995, 34, 4828;
6. V. A. Ung, A. M. W. Cargill Thompson, D. A. Bardwell, D. Gatteschi, J. C Jeffery, F. Totti and M. D. Ward, Inorg. Chem., 1997, 36, 3447.
7. M. D. Ward, Chem. Soc. Rev., 1995, 121.
8. O. Kahn, Molecular Magnetism, VCH, Weinheim, 1993.
9. V. A. Grillo, Z. Sun, K. Folting, D. N. Hendrickson and G. Christou, Chem. Commun., 1996, 2233;
10. V. A. Grillo, M. J. Knapp, J. C. Bollinger, D. N. Hendrickson and G. Christou, Angew. Chem., Int. Ed. Engl., 1996, 35, 1818;
11. H. J. Eppley, H.-L. Tsai, N. de Vries, K. Folting, G. Christou and D. N. Hendrickson, J. Am. Chem. Soc., 1995, 117, 301;
12. M. A. Bolcar, S. M. J. Aubin, K. Folting, D.-N. Hendrickson and G. Christou, Chem. Commun., 1997, 1485.
13. Other examples of 'molecular grids': P. N. W. Baxter, J.-M. Lehn, J. Fischer and M.-T. Youinou, Angew. Chem., Int. Ed. Engl., 1994, 33, 2284;
14. P. N. W. Baxter, J.-M. Lehn, B. O. Kneisel and D. Fenske, Chem. Commun., 1997, 2231;
15. Angew. Chem., Int. Ed. Engl., 1997, 36, 1978;
16. G. S. Hanan, D. Volkmer, U. S. Schubert, J.-M. Lehn, G. Baum and D. Fenske, Angew. Chem., Int. Ed. Engl., 1997, 36, 1842;
17. C. Duan, Z. Liu, X. You, F. Xue and T. C. W. Mak, Chem. Commun., 1997, 381.
18. V. C. M. Smith and J.-M. Lehn, Chem. Commun., 1996, 2733.
19. V. P. Hanot, T. D. Robert, J. Kolnaar, J. G. Haasnoot, J. Reedijk, H. Kooijman and A. L. Spek, J. Chem. Soc., Dulton Trans., 1996, 4275 and refs. therein.
20. (a) T. Otieno, S. J. Rettig, R. C. Thompson and J. Trotter, Inorg. Chem., 1995, 34, 1718;
21. (b) J. Casabó, J. Pons, K. S. Siddiqi, F. Teixidor, E. Molins and C. Miravitlles, J. Chem. Soc., Dalton Trans., 1989, 1401;
22. (c) J. Pons, X. López, J. Casabó, F. Teixidor, A. Caubet, J. Ruis and C. Miravitlles, Inorg. Chim. Acta, 1992, 195, 61;
23. (d) J. Pons, F. J. Sánchez, A. Labarta, J. Casabó, F. Teixidor and A. Caubet, Inorg. Chim. Acta, 1993, 208, 167;
24. (e) M. Munakata, L. P. Wu, M. Yamamoto, T. Kuroda-Sowa, M. Maekawa, S. Kawata and S. Kitagawa, J. Chem. Soc., Dalton Trans., 1995, 4099;
25. (f) P. M. Slangen, P. J. van Koningsbruggen, K. Goubitz, J. G. Haasnoot and J. Reedijk, Inorg. Chem., 1994, 33, 1121.
26. J. C. Jeffery, P. L. Jones, K. L. V. Mann, E. Psillakis, J. A. McCleverty, M. D. Ward and C. M. White, Chem. Commun., 1997, 175.
27. A. J. Amoroso, A. M. W. Cargill Thompson, J. C. Jeffery, P. L. Jones, J. A. McCleverty and M. D. Ward, J. Chem. Soc., Chem. Commun., 1994, 2751;
28. H. Brunner and T. Scheck, Chem. Ber., 1992, 125, 701.
29. J. S. Fleming, E. Psillakis, S. M. Couchman, J. C. Jeffery, J. A. McCleverty and M. D. Ward, J. Chem. Soc., Dalton Trans., 1998, 537.
30. P. L. Jones, A. J. Amoroso, J. C. Jeffery, J. A. McCleverty, E. Psillakis, L. H. Rees and M. D. Ward, Inorg. Chem., 1997, 36, 10.
31. SHELXTL 5.03 program system, Siemens Analytical X-Ray Instruments, Madison, WI, 1995.
32. D. Gatteschi and L. Pardi, Gazz. Chim. Ital., 1993, 123, 231.
33. W. H. Press, B. P. Flannery, S. A. Teukolsky and W. T. Vetterling, Numerical Recipes, Cambridge University Press, 1968.
34. G. M. Smith, J. C. G. LeSurf, R. H. Mitchell and P. C. Riedi, MTT Symposium Proceedings, Orlando, 1995, Rev. Sci. Instrum., 1998, 69, 3924.
35. F. E. Mabbs and D. Collison, Electron paramagnetic resonance of d-transition metal compounds, Elsevier, Amsterdam, 1992, Chs. 7 and 16.
36. P. L. Jones, J. C. Jeffery, J. A. McCleverty and M. D. Ward, Polyhedron, 1997, 16, 1567.
37. K. Singh, J. R. Long and P. Stavropoulos, J. Am. Chem. Soc., 1997, 119, 2942.
38. W. R. Thiel and T. Priermeier, Angew. Chem., Int. Ed. Engl., 1995, 34, 1737;
39. W. R. Thiel, M. Angstl and T. Priermeier, Chem. Ber., 1994, 127, 2373;
40. J. Sieler and H. Hennig, Z. Anorg. Allg. Chem., 1971, 381, 219;
41. Y. Luo, P. G. Potvin, Y.-H. Tse and A. B. P. Lever, Inorg. Chem., 1996, 35, 5445.
42. G. Eaton and M. C. R. Symons, J. Chem. Soc., Faraday Trans. 1, 1988, 84, 3459.
43. D. A. Bardwell, J. C. Jeffery and M. D. Ward, Inorg. Chim. Acta, 1995, 236, 125 and refs. therein.
44. V. C. M. Smith and J.-M. Lehn, Chem. Commun., 1996, 2733.
45. A. Bencini, D. Gatteschi, C. Zanchini, J. G. Haasnoot, R. Prins and J. Reedijk, J. Am. Chem. Soc., 1987, 109, 2926.
46. P. Chaudhuri, I. Karpenstein, M. Winter, M. Lengen, C. Butzlaff, E. Bill, A. X. Trautwein, U. Flörke and H.-J. Haupt, Inorg. Chem., 1993, 32, 888.