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21
-
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33846907796
-
-
note
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3): δ 168.61, 46.10, 44.30, 41.83, 33.37, 31.83, 25.90.
-
-
-
-
22
-
-
33846916883
-
-
note
-
2: C, 32.53; H, 4.64; N, 7.59; S, 8.69. Found C, 32.46; H, 4.87; N, 7.66; S, 8.66%.
-
-
-
-
23
-
-
33846908283
-
-
note
-
-), 1259 w, 1200 w, 1026 m, 823 w.
-
-
-
-
24
-
-
33846930844
-
-
note
-
2 using SHELXTL software [16].
-
-
-
-
25
-
-
33846904982
-
-
Bruker, SHELXTL-PC, Version 5.10, Bruker-Analytical X-ray Services: Madison, WI, 1998.
-
-
-
-
26
-
-
33846931543
-
-
note
-
Crystals of 2 appear to contain certain amount of the acetonitrile-water solvent mixture trapped in the crystal lattice in a severely disordered manner. The solvent could not be reliably modelled, and therefore the Squeeze technique [18] was used to subtract its contribution from the diffraction pattern.
-
-
-
-
28
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-
0001287946
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-
Hu K., Bradshaw J.S., Pastushok V.N., Krakowiak K.E., Dalley N.K., Zhang X.X., and Izatt R.M. J. Org. Chem. 63 (1998) 4786
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Dalley, N.K.5
Zhang, X.X.6
Izatt, R.M.7
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29
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0001542904
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-
Xu C., Hampden-Smith M.J., Kodas T.T., Duesler E.N., Rheingold A.L., and Yap G. Inorg. Chem. 34 (1995) 4767
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Yap, G.6
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