Self-assembly of a water chain with tetrameric and decameric clusters in the channel of a mixed-valence CuICuII complex

Crystal Growth and Design

Volumn 7, Issue 1, 2007, Pages 15-17

  Hu, Ning Hai ^a   Li, Zhi Gang ^a   Xu, Jing Wei ^a   Jia, Heng Qing ^a   Niu, Jia Jia ^a  

^a CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33846475425     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg060641r     Document Type: Article

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41. -1. The resulting yellow crystals of 1, suitable in size for single-crystal X-ray diffraction, were filtered off and dried in air. Yield: 32%.
42. 2 = 0.092 for 5973 reflections with I > 2σ(I). X-ray diffraction data were collected on a Bruker SMART APEX CCD diffractometer with MoKa radiation (λ = 0.71073 Å). Non-hydrogen atoms were refined anisotropically. The hydrogen atoms on the ligands were generated geometrically and refined as riding atoms, and those on the water molecules were positioned from difference Fourier maps and fixed in the refinement.
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