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Volumn , Issue 3, 2007, Pages 417-419

A new synthetic route for the preparation of 1,10-phenanthroline derivatives

a CNRS (France)

Author keywords

1,10 phenanthroline; Cleavage reactions; Heterocycles; Organolithium reagents

Indexed keywords

EID: 33846464979 PISSN: 1434193X EISSN: 10990690 Source Type: Journal
DOI: 10.1002/ejoc.200600772 Document Type: Article

Times cited : (19)

References (16)

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13
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- The oxidation of di- or tetrahydrophenanthroline intermediates resulting from the reaction of 1,10-phenanthroline with an organolithium reagent followed by quenching with water occurs under air but is not very efficient and in addition undefined degradation products are obtained. In this case, the use of an oxidant (MnO2) is necessary to perform clean aromatization, see ref.[4
- [4]

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- 2 led to 1-alky 1-1,10-phenanthrolin-2-one; see: M. R. Johnson, D. Bell, L. Shanaman, Heterocycles 1997, 45, 1059-1069.
- 2 led to 1-alky 1-1,10-phenanthrolin-2-one; see: M. R. Johnson, D. Bell, L. Shanaman, Heterocycles 1997, 45, 1059-1069.

15
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- Full data collection parameters and structural data are available as CIF files. CCDC-615458 (for 5b), -615459 (for 5d), and 615460 (for 7d) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
- Full data collection parameters and structural data are available as CIF files. CCDC-615458 (for 5b), -615459 (for 5d), and 615460 (for 7d) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.

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