Quantitative analysis of paeoniflorin from Paeonia lactiflora using 1H-NMR

Natural Product Sciences

Volumn 12, Issue 4, 2006, Pages 237-240

  Yoo, Jong Su ^a   Song, Myoung Chong ^a   Ahn, Eun Mi ^b   Lee, Youn Hyung ^a   Rho, Yeong Deok ^a   Baek, Nam In ^a  

^a Kyung Hee University   (South Korea)

^b Daegu Haany University   (South Korea)

Author keywords

1H NMR; Paeonia lactiflora; Paeoniflorin; Quantitative analysis

Indexed keywords

2,4,6 TRIHYDROXYBENZALDEHYDE; BENZALDEHYDE DERIVATIVE; PAEONIA LACTIFLORA EXTRACT; PAEONIFLORIN; UNCLASSIFIED DRUG;

ARTICLE; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PAEONIA; PROTON NUCLEAR MAGNETIC RESONANCE; QUANTITATIVE ANALYSIS; SPECTROMETER;

EID: 33846408305     PISSN: 12263907     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (22)

1. Aimi, N., Inaba, M., Watanabe, M., and Shibata, S., Peoniflorin, a glucoside of Chinese paeony root. Tetrahedron, 25(9), 1825-1838 (1969).
2. 1H-NMR. Phytochemical analysis, 15(5), 325-330 (2004a).
3. 1H-nuclear magnetic resonance spectroscopy. Analytica Chimica Acta, 512(1), 141-147 (2004b).
4. Hsu, F.L., Lai, C.W., and Cheng, J.T., Antihyperglycemic effects of paeoniflorin and 8-debenzoylpaeoniflorin, glucosides from the root of Paeonia lactiflora. Planta medico, 63(4), 323-325 (1997).
5. Ikeda, N., Fukuda, T., Jyo, H., Shimada, Y., Murakami, N., Saka, M., and Yoshikawa, M., Quantitative analysis of monoterpene glycosides constituents of Paeoniae Radix by means of high performance liquid chromatography. Comparative characterization of the external figures, processing method and the cultivated areas. Yakugaku Zasshi, 116(2), 138-147 (1996).
6. Kaneda, M., Iitaka, Y., and Shibata, S., Absolute structure of paeoniflorin, albiflorin, oxypaeoniflorin, and benzoylpaeoniflorin isolated from Chinese paeony root. Tetrahedron, 28(16), 4309-4317 (1972).
7. Kang, S.S., Kim, J.S., Yun-Choi, H.S., and Han, B.H., Phytochemical studies on Paeoniae Radix. Korean Journal of Pharmacognosy, 24(3), 247-50 (1993).
8. Kang, S.S., Shin, K.H., and Chi, H.J., Galloylpaeoniflorin, a new acylated monoterpene glucoside from Paeony root. Archives of Pharmacal Research, 14(1), 52-54 (1991).
9. Kim, K.J., You, O.J., Jeong, Y.S., Park, S.D., Shin, J.H., Hwang, H.B., and Choi, B.S., Changes of root yield and paeoniflorin content by cultivated years in Paeonia lactiflora PALLS. Korean Journal of Medicinal Crop Science, 4(1), 168-73 (1996).
10. Kim, K.S. and Kim, H.C., Analytical method for the determination of standard compounds in oriental medicine materials listed in the Korean Pharmacopoeia (KPVIII). Korean Journal of Crop Science, 49(1), 117-145 (2004).
11. Kim, N.S., Park, K.R., Park, I.S., and Park, Y.H., Application of novel HPLC method to the analysis of regional and seasonal variation of the active compounds in Paeonia lactiflora. Food Chemistry, 96(3), 496-502 (2006).
12. Lee, S.C., Kwon, Y.S., Son, K.H., Kim, H.P., and Heo, M.Y., Antioxidative constituents from Paeonia lactiflora. Archives of Pharmacal Research, 28(7), 775-783 (2005).
13. Liu, D.F., Wei, W., and Song, L.H., Protective effect of paeoniflorin on immunological liver injury induced by bacillus calmette-guerin plus lipopolysaccharide: modulation of tumor necrosis factor-alpha and interleukin-6 mRNA. Clinical and Experimental Pharmacology and Physiology, 33(4), 332-339 (2006).
14. Malz, F. and Jancke, H., Validation of quantitative NMR. Journal of pharmaceutical and biomedical analysis, 38(5), 813-823 (2005).
15. Son, D.J. and Park, Y.H., Effect of extract from Paeonia radix on rabbit platelets. The Korean Society of Food Science and Nutrition, 31(3), 511-515 (2002).
16. 1H-NMR spectrometry. Journal of Korean Society for Applied Biological Chemistry, 48(3), 267-272, (2005).
17. Sugishita, E., Amagaya, S., and Ogihara, Y., Studies on the combination of Glycyrrhizae Radix in Shakuyakukanzo-To. Journal of pharmacobiodynamics, 7(7), 427-435 (1984).
18. Okamoto, M. and Noguchi, M., Evaluation of 3-cyanopropyltrichlorosilane treated thin layer chromatographic plates. Application to analysis of paeoniflorin in paeony roots. Yakugaku Zasshi, 106(9), 837-839 (1986).
19. Wu, H.K. and Sheu, S.J., Capillary electrophoretic determination of the constituents of Paeoniae Radix. Journal of Chromatography A, 753(1), 139-146 (1996).
20. Yamahara, J., Yamada, T., Kimura, H., Sawada, T., and Fujimura, H., Anti-allergic principles in "Shoseiryu-To" anti-inflammatory properties of paeoniflorin and its derivatives. Journal of pharmacobio-dynamics, 5(11), 921-929 (1982).
21. Ye, J., Duan, H., Yang, X., Yan, W., and Zheng, X., Anti-thrombosis effect of paeoniflorin: evaluated in a photochemical reaction thrombosis model in vivo. Planta Medica, 67(8), 766-767 (2001).
22. Yu, J., Elix, J.A., and Iskander, M.N., Lactiflorin, a monoterpene glycoside from peony root. Phytochemistry, 29(12), 3859-3863 (1990).