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note
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-1. A total of 6638 data were collected and merged to give 1595 unique reflections of which 1539 were considered to be observed [I > 2σ(I)]. Final R values (0.0228, wR = 0.0502, S = 1.193) were obtained for 1595 reflections with I > 2σ(I) and a total of 1 1 8 parameters.
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