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note
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-1 in air.
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34
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33645280839
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note
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-1. A total of 3593 data were collected and merged to give 857 unique reflections of which 792 were considered to be observed [I > 2σ(I)]. The structure was solved using weight-atom methods and refined using SHELXTL software. All the non-hydrogen atoms were assigned anisotropically. Final R values (R = 0.0271, wR = 0.0643, S = 1.084) were obtained for 857 reflections with I > 2σ(I) and a total of 42 parameters. CCDC Number for 1 294470.
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