Synthesis and characterization of osmium polyhydrides. X-ray crystal structures of (C5Me5)OsH5 and (C 5Me5)2Os2H4

Organometallics

Volumn 26, Issue 1, 2007, Pages 160-166

  Gross, Christopher L ^a   Girolami, Gregory S ^a  

^a UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

HYDRIDE LIGANDS; OSMIUM POLYHYDRIDES; POLYHYDRIDE STRUCTURE; TETRAHYDRIDE SALT;

HYDRIDES; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; SYNTHESIS (CHEMICAL); THERMAL EFFECTS; X RAY CRYSTALLOGRAPHY;

OSMIUM COMPOUNDS;

EID: 33846263427     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om060920b     Document Type: Article

References (36)

1. Heinekey, D. M.; Oldham, W. J., Jr. Chem. Rev. 1993 93, 913-926.
2. Heinekey, D. M.; Millar, J. M.; Koetzle, T. F.; Payne, N. G.; Zilm, K. W. J. Am. Chem. Soc. 1990, 112, 909-919.
3. Zilm, K. W.; Heinekey, D. M.; Millar, J. M.; Payne, N. G.; Neshyba, S. P.; Duchamp, J. C.; Szczyrba, J. J. Am. Chem. Soc. 1990, 112, 920929.
4. Clapham, S. E.; Hadzovic, A.; Morris, R. H. Coord. Chem. Rev. 2004, 248, 2201-2237.
5. Heinekey, D. M.; Lledos, A.; Lluch, J. M. Chem. Soc. Rev. 2004, 33, 175-182.
6. Maseras, F.; Lledos, A.; Clot, E.; Eisenstein, O. Chem. Rev. 2000, 100, 601-636.
7. Sabo-Etienne, S.; Chaudret, B. Coord. Chem. Rev. 1998, 178, 381-407.
8. Hlatky, G. G.; Crabtree, R. H. Coord. Chem. Rev. 1985, 65, 1-48.
9. Herrmann, W. A.; Theiler, H. G.; Kiprof, P.; Tremmel, J.; Blom, R. J. Organomet. Chem. 1990, 395, 69-84.
10. Gilbert, T. M.; Hollander, F. J.; Bergman, R. G. J. Am. Chem. Soc. 1985, 107, 3508-3516.
11. Moreno, B.; Sabo-Etienne, S.; Chaudret, B.; Rodriguez-Fernandez, A.; Jalon, F.; Trofimenko, S. J. Am. Chem. Soc. 1994, 116, 2635-2636.
12. Moreno, B.; Sabo-Etienne, S.; Chaudret, B.; Rodriguez-Fernandez, A.; Jalon, F.; Trofimenko, S. J. Am. Chem. Soc. 1995, 117, 7441-7451.
13. Gründemann, S.; Ulrich, S.; Limbach, H.-H.; Golubev, N. S.; Denisov, G. S.; Epstein, L. M.; Sabo-Etienne, S., Chaudret, B. Inorg. Chem. 1999, 38, 2550-2551.
14. Johnson, T. J.; Coan, P. S.; Caulton, K. G. Inorg. Chem. 1993, 32, 4594-4599.
15. Aneetha, H.; Tenorio, M. J.; Puerta, M. C.; Valerga, P. J. Organomet. Chem. 2002, 663, 151-157.
16. Gross, C. L.; Wilson, S. R.; Girolami, G. S. J. Am. Chem. Soc. 1994, 116, 10294-10295.
17. Gross, C. L.; Brumaghim, J. L.; Girolami, G. S. Organometallics, in press.
18. Shima, T.; Suzuki, H. Organometallics 2005, 24, 3939-3945.
19. Bayse, C. A.; Couty, M.; Hall, M. B. J. Am. Chem. Soc. 1996, 118, 8916-8919.
20. Gusev, D. G.; Berke, H. Chem. Ber. 1996, 129, 1143-1155.
21. Hamilton, D. G.; Crabtree, R. H. J. Am. Chem. Soc. 1988, 110, 4126-4133.
22. Desrosiers, P. J.; Cai, L.; Lin, Z.; Richards, R.; Halpern, J. J. Am. Chem. Soc. 1991, 113, 4173-4184.
23. For similar compounds, see: Gross, C. L.; Girolami, G. S. Organometallics 2006, 25, 4792-4798.
24. Gross, C. L.; Girolami, G. S. Organometallics 1996, 15, 5359-5367.
25. Lin, Z. Y.; Hall, M. B. Coord. Chem. Rev. 1994, 135/136, 845-879.
26. Cooper, R. L.; Green, M. L. H.; Moelwyn-Hughes, J. T. J. Organomet. Chem. 1965, 3, 261-268.
27. Lin, Z. Y.; Hall, M. B. Organometallics 1992, 11, 3801-3804.
28. Gelabert, R.; Moreno, M.; Lluch, J. M.; Lledos, A. Organometallics 1997, 16, 3805-3814.
29. Suzuki, H.; Omori, H.; Lee, D. H.; Yoshida, Y.; Fukushima, M.; Tanaka, M.; Moro-oka, Y. Organometallics 1994, 13, 1129-1146.
30. Ohki, Y.; Suzuki, H. Angew. Chem., Int. Ed. 2000, 39, 3120-3122.
31. Suzuki, H.; Omori, H.; Lee, D. H.; Yoshida, Y.; Moro-oka, Y. Organometallics 1988, 7, 2243-2245.
32. Marsh, R. E. Organometallics 1989, 8, 1583-1584.
33. 18
34. Koga, N.; Morokuma, K. J. Mol. Struct. 1993, 300, 181-189.
35. Luetkens, M. L.; Sattelberger, A. P.; Murray, H. H.; Basil, D. J.; Fackler, J. P. Inorg. Synth. 1989, 26, 7-12.
36. For a description of the crystallographic programs and procedures used, see: Brumaghim, J. L.; Priepot, J. G.; Girolami, G. S. Organometallics 1999, 18, 3139-2144.