Freezing characteristics of acrylamide-based aqueous solution used for the preparation of supermacroporous cryogels via cryo-copolymerization

Chemical Engineering Science

Volumn 62, Issue 5, 2007, Pages 1334-1342

  He, Xingjiao ^a   Yao, Kejian ^a   Shen, Shaochuan ^a   Yun, Junxian ^a  

^a ZHEJIANG UNIVERSITY OF TECHNOLOGY   (China)

Author keywords

Freezing curve; Freezing point temperature; Initial solvent crystallization temperature; Monolith; Solvent freezing crystallization; Supermacroporous cryogel

Indexed keywords

COOLING; COPOLYMERIZATION; FREEZING; GELS; SOLUTIONS; SYNTHESIS (CHEMICAL);

FREEZING CURVE; FREEZING POINT TEMPERATURE; INITIAL SOLVENT CRYSTALLIZATION TEMPERATURE; SOLVENT FREEZING CRYSTALLIZATION; SUPERMACROPOROUS CRYOGELS;

CRYSTALLIZATION;

COOLING; COPOLYMERIZATION; CRYSTALLIZATION; FREEZING; GELS; SOLUTIONS; SYNTHESIS (CHEMICAL);

EID: 33846229691     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ces.2006.11.027     Document Type: Article

References (22)

1. Akyurt M., Zaki G., and Habeebullah B. Freezing phenomena in ice-water systems. Energy Conversion and Management 43 (2002) 1773
2. Arvidsson P., Plieva F.M., Savina I.N., Lozinsky V.I., Fexby S., Bülow L., Galaev I.Y., and Mattiasson B. Chromatography of microbial cells using continuous supermacroporous affinity and ion-exchange columns. Journal of Chromatography A 977 (2002) 27
3. Arvidsson P., Plieva F.M., Lozinsky V.I., Galaev I.Y., and Mattiasson B. Direct chromatographic capture of enzyme from crude homogenate using immobilized metal affinity chromatography on a continuous supermacroporous adsorbent. Journal of Chromatography A 986 (2003) 275
4. Ayel V., Lottin O., Popa E., and Peerhossaini H. Using undercooling to measure the freezing points of aqueous solutions. International Journal of Thermal Sciences 44 (2005) 11
5. Ayel V., Lottin O., Faucheux M., Sallier D., and Peerhossaini H. Crystallisation of undercooled aqueous solutions: experimental study of free dendritic growth in cylindrical geometry. International Journal of Heat and Mass Transfer 49 (2006) 1876
6. Belavtseva E.M., Titova E.F., Lozinsky V.I., Vainerman E.S., and Rogozhin S.V. Study of cryostructurization of polymer systems V. Electron microscopic studies of cross-linked polyacrylamide cryogels. Colloid and Polymer Science 262 (1984) 775
7. Chen X.D., and Chen P. Freezing of aqueous solution in a simple apparatus designed for measuring freezing point. Food Research International 29 (1996) 723
8. Dainiak M.B., Kumar A., Plieva F.M., Galaev I.Y., and Mattiasson B. Integrated isolation of antibody fragments from microbial cell culture fluids using supermacroporous cryogels. Journal of Chromatography A 1045 (2004) 93
9. Kumar A., Plieva F.M., Galaev I.Y., and Mattiasson B. Affinity fractionation of lymphocytes using a monolithic cryogel. Journal of Immunological Methods 283 (2003) 185
10. Kumar A., Bansal V., Andersson J., Roychoudhury P.K., and Mattiasson B. Supermacroporous cryogel matrix for integrated protein isolation: immobilized metal affinity chromatographic purification of urokinase from cell culture broth of a human kidney cell line. Journal of Chromatography A 1003 (2006) 35
11. Lottin O., and Epiard C. Dependence of the thermodynamic properties of ice slurries on the characteristics of marketed antifreezes. International Journal of Refrigeration 24 (2001) 455
12. Lozinsky V.I., Vainerman E.S., Titova E.F., Belavtseva E.M., and Rogozhin S.V. Study of cryostructurization of polymer systems IV. Cryostructurization of the system: solvent-vinyl monomer-divinyl monomer-initiator of polymerization. Colloid and Polymer Science 262 (1984) 769
13. Lozinsky V.I., Vainerman E.S., Ivanova S.A., Titova E.F., Shtil'Man M.I., and Belavtseva E.M. Study of cryostructurization of polymer systems. VI. The influence of the process temperature on the dynamics of formation and structure of cross-linked polyacrylamide cryogels. Acta Polymerica 37 (1986) 142
14. Lozinsky V.I., Morozova S.A., and Vainerman E.S. Study of cryostructurization of polymer systems. VIII. Characteristic features of the formation of crosslinked poly(acryl amide) cryogels under different thermal conditions. Acta Polymerica 40 (1989) 8
15. Okawa S., Saito A., and Minami R. The solidification phenomenon of the supercooled water containing solid particles. International Journal of Refrigeration 24 (2001) 108
16. Okawa S., Saito A., and Suto H. The experimental study on freezing of supercooled water using metallic surface. International Journal of Refrigeration 25 (2002) 514
17. Persson P., Baybak O., Plieva F.M., Galaev I.Y., Mattiasson B., Nilsson B., and Axelsson A. Characterization of a continuous supermacroporous monolithic matrix for chromatographic separation of large bioparticles. Biotechnology and Bioengineering 88 (2004) 224
18. Plieva F.M., Andersson J., Galaev I.Y., and Mattiasson B. Characterization of polyacrylamide based monolithic columns. Journal of Separation Science 27 (2004) 828
19. Plieva F.M., Savina I.N., Deraz S., Andersson J., Galaev I.Y., and Mattiasson B. Characterization of supermacroporous monolithic polyacrylamide based matrices designed for chromatography of bioparticles. Journal of Chromatography B 807 (2004) 129
20. Williams S.L., Eccleston M.E., and Slater N.K.H. Affinity capture of a biotinylated retrovirus on macroporous monolithic adsorbents: towards a rapid single-step purification process. Biotechnology and Bioengineering 89 (2005) 783
21. Yao K.J., Yun J.X., Shen S.C., Wang L.H., He X.J., and Yu X.M. Characterization of a novel continuous supermacroporous monolithic cryogel embedded with nanoparticles for protein chromatography. Journal of Chromatography A 1109 (2006) 103
22. Yao K.J., Shen S.C., Yun J.X., Wang L.H., He X.J., and Yu X.M. Preparation of polyacrylamide-based supermacroporous monolithic cryogel beds under freezing-temperature variation conditions. Chemical Engineering Science 61 (2006) 6701