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We exclusively used anhydrous solvents for this study since the solvents are purer than other grades of general solvents
-
We exclusively used anhydrous solvents for this study since the solvents are purer than other grades of general solvents.
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24
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33846072644
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The corresponding carboxylic acids were obtained in moderate yields when using 0.07 eq of bromine
-
The corresponding carboxylic acids were obtained in moderate yields when using 0.07 eq of bromine.
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25
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33846081170
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Since the boiling point of 15 is not so high, remained 15 in the crude product was thought to be evaporated under reduced pressure with a vacuum pump.
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Since the boiling point of 15 is not so high, remained 15 in the crude product was thought to be evaporated under reduced pressure with a vacuum pump.
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26
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33846108872
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The equivalent indicates the amount of hydrogen bromide in the hydrobromic acid
-
The equivalent indicates the amount of hydrogen bromide in the hydrobromic acid.
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27
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33846093154
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Since the reaction mixture was tarry and the product 12 was obtained only in 33% yield when using 11 and 0.2 eq of hydrobromic acid, 0.1 eq of hydrobromic acid was exclusively used for aliphatic aldehydes.
-
Since the reaction mixture was tarry and the product 12 was obtained only in 33% yield when using 11 and 0.2 eq of hydrobromic acid, 0.1 eq of hydrobromic acid was exclusively used for aliphatic aldehydes.
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28
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5644262720
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