Determination of active ingredients of spatholobus suberectus dunn and its medicinal preparations by capillary electrophoresis with electrochemical detection

Journal of Liquid Chromatography and Related Technologies

Volumn 30, Issue 1, 2007, Pages 59-71

  Tang, Zhuxing ^a   Zeng, Yikun ^b   Zhou, Yun ^b   He, Pingang ^b   Fang, Yuzhi ^b   Zang, Shuliang ^c  

^a SHENYANG LIGONG UNIVERSITY   (China)

^b EAST CHINA NORMAL UNIVERSITY   (China)

^c LIAONING UNIVERSITY   (China)

Author keywords

Capillary electrophoresis; Electrochemical detection; Spatholobus suberectus dunn

Indexed keywords

CAPILLARY ELECTROPHORESIS; CARBON DISK ELECTRODE; ELECTROCHEMICAL DETECTION; SEPARATION VOLTAGE; SPATHOLOBUS SUBERECTUS DUNN;

ELECTROCHEMISTRY; ELECTRODES; ELECTROPHORESIS; PH EFFECTS;

ORGANIC COMPOUNDS;

BORIC ACID; BUFFER; EMODIN; EPICATECHIN; PLANT EXTRACT; PROTOCATECHUIC ACID; RHEIN; SPATHOLOBUS SUBERECTUS DUNN EXTRACT; SYRINGIC ACID; UNCLASSIFIED DRUG; VANILLIC ACID;

ARTICLE; CAPILLARY ELECTROPHORESIS; CONCENTRATION (PARAMETERS); DRUG DETERMINATION; DRUG ISOLATION; DRUG SYNTHESIS; ELECTRIC POTENTIAL; ELECTROCHEMICAL DETECTION; ELECTRODE; LEGUME; PH; SPATHOLOBUS SUBERECTUS DUNN;

SPATHOLOBUS;

EID: 33845809566     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070601034279     Document Type: Article

References (18)

1. Li, L.N. Biologically active components from traditional Chinese medicines. Pure Appl. Chem. 1998, 70, 547-554.
2. Zhong Yao Jian Ding Xue; Shanghai Science and Technology Press: Shanghai, 2000; 278-280.
3. Cui, Y.J.; Liu, P.; Chen, R.Y. Studies On the active constituents in vine stem of spatholobus suberectus. China J. Chinese Materia. Med. 2005, 30, 121-123 (Chinese).
4. Yan, Q.X.; Li, P.; Hu, A.M. Studies on the chemical constituents of Spatholobus Suberectus Dunn. Chinese Tradit. Herb. Drugs 2003, 34, 876-878 (Chinese).
5. Yan, Q.X.; Li, P. Study on HPLC fingerprint of Caulis Spatholobi. Chinese Tradit. Herb. Drugs 2004, 35, 556-559 (Chinese).
6. Jovanovic, S.V.; Steenken, S.; Hara, Y.; Simic, M.G. Reduction potentials of flavonoid and model phenoxyl radicals. Which ring in flavonoids is responsible for antioxidant activity? J. Chem. Soc. Perkin Trans. 1996, 2, 2497-2504.
7. Hertog, M.G.L.; Hollman, P.C.H.; van de Putte, B. Content of potentially anticarcinogenic flavonoids of tea infusions, wines, and fruit juices. J. Agric. Food Chem. 1993, 41, 1242-1246.
8. Briviba, K.; Sies, H. Natural Antioxidant in Human Health and Disease; Frei, B., Ed.; Academic Press: New York, 1994; 107-112.
9. Hollman, P.C.H.; Hertog, M.G.L.; Katan, M.B. Analysis and health effects of flavonoids. Food Chem. 1996, 57, 43-46.
10. Rice-Evans, C.A.; Miller, N.J.; Paganga, G. Structure-antioxidant activity relationships of flavonoids and phenolic acids. Free Radical Bio. Med. 1996, 20, 933-956.
11. Chen, Y.J.; Shiao, M.S.; Hsu, M.L.; Tsai, T.H.; Wang, S.Y. Effect of caffeic acid phenethyl ester, an antioxidant from propolis, on inducing apoptosis in human leukemic HL-60 cells. J. Agric. Food Chem. 2001, 49, 5615-5619.
12. Chen, G.; Zhang, L.Y.; Wu, X.L.; Ye, J.N. Determination of mannitol and three sugars in Ligustrum lucidum Ait by capillary electrophoresis with electrochemical detection. Anal. Chim. Acta 2005, 530, 15-21.
13. Cao, Y.H.; Lou, C.G.; Fang, Y.Z.; Ye, J.N. Determination of active ingredients of Rhododendron dauricum L. by capillary electrophoresis with electrochemical detection. J. Chromatogr. A 2001, 943, 153-157.
14. Wang, A.F.; Zhou, Y.; Wu, F.; He, P.G.; Fang, Y.Z. Determination of active ingredients in Huangdan Yinchen Keli by CZE with amperometric detection. J. Pharm. Biomed. Anal 2004, 35, 959-964.
15. Wang, Q.J.; Ding, F.; Li, H.; He, P.G.; Fang, Y.Z. Determination of hydrochlorothiazide and rutin in Chinese herb medicines and human urine by capillary zone electrophoresis with amperometric detection. J. Pharm. Biomed. Anal. 2003, 30, 1507-1514.
16. Tang, Z.X.; Zhou, Y.; Zeng, Y.K.; Zang, S.L.; He, P.G.; Fang, Y.Z. Determination of active ingredients of Ilex Purpurea Hassk and its medicinal preparations by capillary electrophoresis with electrochemical detection. J. Pharm. Biomed. Anal. 2006, 40, 484-489.
17. Fang, Y.Z.; Gong, F.Y.; Liu, X.F.; Fang, X.M.; Ye, J.N. Determination of priority phenols in wastewater by capillary electrophoresis with electrochemical detection. Chinese J. Anal. Chem. 1998, 26, 694-697.
18. Fu, C.G.; Song, L.N.; Fang, Y.Z. Determination of adenosine phosphate by co-electroosmotic capillary electrophoresis with amperometric detection. Anal. Chim. Acta 1999, 399, 259-263.