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33845688926
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note
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2).
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18
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37049086529
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33845706168
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note
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2; (5) Otera's distannoxane-promoted transesterification; (6) BOP, DIPEA, DMAP, DMF.
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24
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0035594725
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2O in THF in the presence of DMAP (cat) at room temperature for 5 h (Wille, G.; Steglich, W. Synthesis 2001, 5, 759).
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33845711262
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Pirkle (R,R)-WHELK-01 column: eluant: hexane/propan-2-ol/diethylamine 20:5:0.1; flow: 1 mL/min.
-
-
-
-
47
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0344442241
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53
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33845694064
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note
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2 = 0.1242) for 3134 observed reflections and 245 parameters. Supplementary crystallographic data were deposited as CCDC 622273 with the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK.
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