New hybrid diphosphates Ln2(NH2(CH2) 2NH2)(HP2O7)2·4 H2O (Ln=Eu, Tb, Er): Synthesis, single crystal and powder X-ray crystal structure

Zeitschrift fur Kristallographie

Volumn 221, Issue 12, 2006, Pages 788-794

  Capitelli, Francesco ^a   El Bali, Brahim ^b   Essehli, Rachid ^d   Lachkar, Mohammed ^b   Da Silva, Iván ^c  

^a CNR   (Italy)

^b SIDI MOHAMED BEN ABDELLAH UNIVERSITY   (Morocco)

^c UNIVERSIDAD DE LA LAGUNA   (Spain)

^d NONE

Author keywords

Diphosphate; Ethylenediamine; Hydrogen bond; Lanthanide; Powder diffraction structure analysis; Single crystal structure analysis; X ray diffraction

Indexed keywords

EID: 33845655997     PISSN: 00442968     EISSN: None     Source Type: Journal    
DOI: 10.1524/zkri.2006.221.12.788     Document Type: Article

References (22)

1. Altomare, A.; Giacovazzo, C.; Guagliardi, A.; Moliterni, A. G. G.; Rizzi, R.; Werner, P.-E.: New techniques for indexing: N-TREOR in EXPO. J. Appl. Cryst. 33 (2000) 1180-1186.
2. Altomare, A.; Caliandro, R.; Camalli, M.; Cuocci, C.; Giacovazzo, C.; Moliterni, A. G. G.; Rizzi, R.: Automatic structure determination from powder data with EXPO2004. J. Appl. Cryst. 37 (2004) 1025-1028.
3. Altomare, A.; Burla, M. C.; Camalli, M.; Cascarano, G. L.; Giacovazzo, C.; Guagliardi, A.; Moliterni, A. G.; Polidori, G.; Spagna, R.: SIR97: a new tool for crystal determination and refinement. J. Appl. Crystallogr. 32 (1999) 115-119.
4. Bondi, A.: Van der Waals volumes and radii. J. Phys. Chem. 68 (1964) 441-451.
5. Brown, I. D.; Altermatt, D.: Bond-Valence Parameters Obtained from a Systematic Analysis of the Inorganic Crystal Structure Database. Acta Crystallogr. B41 (1985) 244-247.
6. Duisenberg, A. J. M.; Kroon-Batenburg, L. M. J.; Schreurs, A. M. M.: An intensity evaluation method: EVAL-14. J. Appl. Cryst. 36 (2003) 220-229.
7. Durif, A.: Crystal Chemistry of condensed phosphates. Plenum Press, New York, 1995.
8. 2O. Z. Kristallogr. 220 (2005) 25-30.
9. 2O] [Me = Co, Ni]: X-ray crystal structure and vibrational spectroscopy. Z. Kristallogr. 221 (2006) 649-655.
10. Gharbi, A.; Jouini, A.; Averbuch-Pouchot, M. T.; Durif, A.: Ethylenediammonium bis[Copper(II) Monohydrogendiphosphate Ethylenediamine] Trihydrate. J. Sol. State Chem. 111 (1994) 330-337.
11. Inorganic Crystal Structure Database. Version 2005-2. Fachinformationszentrum Karlsruhe, Germany.
12. Madsen, I. C.; Hill, R. J.: Collection and analysis of powder diffraction data with near-constant counting statistics. J. Appl. Cryst. 27 (1994) 385-392.
13. Nardelli, M.: PARST95 - an update to PARST: a system of Fortran routines for calculating molecular structure parameters from the results of crystal structure analyses. J. Appl. Cryst. 28 (1995) 659.
14. Ni, Y.; Hughes, J. M., Mariano, A. N.: Crystal chemistry of the monazite and xenotime structures. American Mineralogist 80 (1995) 21-26.
15. Pierro, C.; Capitelli, F.: Inorganic phosphates investigation by Support Vector Machine. Lect. Notes Comp. Sci. 3044 (2004) 338-349.
16. Reinert, P.; Marier, B.; Patarin, J.: Synthesis and characterization of the new microporous gallophosphate Mu-8. Microporous and Mesoporous Materials 39 (2000) 509-517.
17. Rodriguez-Carvajal, J.: Recent Developments of the Program FULL-PROF. Commission on Powder Diffraction (IUCr). Newsletter 26 (2001) 12-19.
18. 2: a supramolecular three-dimensional hydrogen-bonding network. Acta Cryst. C55 (1999) 921-923.
19. Sheldrick, G. M.: SADABS, Absorption Correction Program. University of Göttingen, Germany, 1996.
20. Sheldrick, G. M.: SHELXL-97. Program for the Refinement of Crystal Structures. University of Gottingen, Germany, 1997.
21. 2O (Ln = Gd, Tb, Yb). Z. Kristallogr. 221 (2006) 173-177.
22. 2O. J. Sol. State Chem. 148 (1999) 450-454.