Sulfur-bonded 2-methylthiopyridine (2-MeSpy) complex of iridium(III). Crystal structure of [Cp*IrI 2-(2-MeSpy-κS)] (Cp* = η 5-C 5Me 5)

Bulletin of the Chemical Society of Japan

Volumn 79, Issue 12, 2006, Pages 1897-1899

  Sekioka, Yusuke ^a   Suzuki, Takayoshi ^a  

^a OSAKA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

DISSOCIATION EQUILIBRIUM; METAL IONS; THIOANISOLE COMPLEX;

BONDING; COMPLEXATION; CRYSTAL STRUCTURE; DISSOCIATION; INFRARED SPECTROSCOPY; IRIDIUM; X RAY CRYSTALLOGRAPHY;

SULFUR;

2 METHYLTHIOPYRIDINE; ANISOLE DERIVATIVE; CADMIUM CHLORIDE; CYCLOPENTADIENE DERIVATIVE; METAL ION; METHYL IODIDE; PYRIDINE DERIVATIVE; SULFUR;

ARTICLE; CRYSTAL STRUCTURE; DISSOCIATION; INFRARED SPECTROSCOPY; SOLID STATE; X RAY CRYSTALLOGRAPHY;

EID: 33845598011     PISSN: 00092673     EISSN: 13480634     Source Type: Journal    
DOI: 10.1246/bcsj.79.1897     Document Type: Article

References (31)

1. Z. Dori, R. F. Ziolo, Chem. Rev. 1973, 73, 247;
2. J. Strähle, Comments Inorg. Chem. 1985, 4, 295.
3. J. Du Bois, C. S. Tomooka, J. Hong, E. M. Carreira, Acc. Chem. Res. 1997, 30, 364;
4. C. A. Grapperhaus, B. Mienert, E. Bill, T. Weyhermüller, K. Wieghardt, Inorg. Chem. 2000, 39, 5306;
5. M. Tsuchimoto, N. Yoshioka, S. Ohba, Eur. J. Inorg. Chem. 2001, 1045.
6. B. C. Lane, J. W. McDonald, V. G. Myers, F. Basolo, R. G. Pearson, J. Am. Chem. Soc. 1971, 93, 4934;
7. E. D. Johnson, F. Basolo, Inorg. Chem. 1977, 16, 554.
8. W. Rigby, P. M. Bailey, J. A. McCleverty, P. M. Maitlis, J. Chem. Soc., Dalton Trans. 1979, 371;
9. C.-W. Chang, G.-H. Lee, Organometallics 2003, 22, 3107;
10. K. S. Singh, C. Thöne, M. R. Kollipara, J. Organomet. Chem. 2005, 690, 4222.
11. H. Nagao, T. Kikuchi, M. Inukai, A. Ueda, T. Oi, N. Suzuki, M. Yamasaki, Angew. Chem., Int. Ed. 2006, 45, 3131.
12. T. Suzuki, A. G. Dipasquale, J. M. Mayer, J. Am. Chem. Soc. 2003, 125, 10514.
13. Y. Sekioka, S. Kaizaki, J. M. Mayer, T. Suzuki, Inorg. Chem. 2005, 44, 8173.
14. M. R. Churchill, S. A. Julis, Inorg. Chem. 1979, 18, 1215.
15. 2] was believed to be correct.
16. A. Mertens, K. Lammertsma, M. Arvanaghi, G. A. Olah, J. Am. Chem. Soc. 1983, 105, 5657.
17. K. M. Rao, C. L. Day, R. A. Jacobson, R. J. Angelici, Inorg. Chem. 1991, 30, 5046.
18. M. Valderrama, R. Contreras, V. Arancibia, D. Boys, J. Organomet. Chem. 2001, 620, 256.
19. S. Ye, W. Kaim, M. Albrecht, F. Lissner, T. Schleid, Inorg. Chim. Acta 2004, 357, 3325.
20. M. Lissel, S. Schmidt, B. Neumann, Synthesis 1986, 382;
21. N. Furukawa, F. Takahashi, T. Kawai, K. Kishimoto, S. Ogawa, S. Oae, Phosphorus, Sulfur 1983, 16, 167.
22. K. Nakamoto, Infrared and Raman Spectra of Inorganic and Coordination Compounds, 5th ed., John Wiley & Sons, New York, U.S.A., 1997, Part B, p. 23;
23. T. Suzuki, M. Kita, K. Kashiwabara, J. Fujita, Bull. Chem. Soc. Jpn. 1990, 63, 3434.
24. J. Vicente, M.-T. Chicote, C. Rubio, Chem. Ber. 1996, 129, 327;
25. J. Vicente, M.-T. Chicote, S. Huertas, M. C. R. de Arellano, P. G. Jones, Eur. J. Inorg. Chem. 1998, 511.
26. A. J. Deeming, M. N. Meah, P. A. Bates, M. B. Hursthouse, Inorg. Chim. Acta 1988, 142, 37;
27. G. F. de Sousa, C. A. L. Filgueiras, Trans. Met. Chem. 1990, 15, 290.
28. T. Higashi, Shape, Rigaku Corporation, Akishima, Tokyo, 1999.
29. A. C. T. North, D. C. Phillips, F. S. Mathews, Acta Crystallogr., Sect. A 1968, 24, 351.
30. A. Altomare, G. Cascarano, C. Giacovazzo, A. Guagliardi, M. Burla, G. Polidori, M. Camalli, J. Appl. Crystallogr. 1994, 27, 435.
31. G. M. Sheldrich, SHELXL97, University of Göttingen, Germany, 1997.