메뉴 건너뛰기




Volumn 9, Issue 12, 2006, Pages 1293-1296

Terminal ligand effect on the structure variation of Copper(II) complexes

Author keywords

Bis(3,5 dimethylpyrazolyl)methane; Copper(II) complex; Crystal structure; Terephthalic acid; Tris(pyrazolyl)methane

Indexed keywords


EID: 33750956743     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2006.08.002     Document Type: Article
Times cited : (15)

References (21)
  • 10
    • 33750937943 scopus 로고    scopus 로고
    • note
    • 2ta (1.0 mmol, 166.1 mg) and 10.0 mL water was stirred for 2 h at room temperature. Then 10.0 mL water solution of tpm (1.0 mmol, 214.0 mg) was added and refluxed 2 h. The mixture was cooled and filtered. Blue crystals suitable for X-ray structure analysis were obtained by slow evaporation of the filtrate for about 10 days in 42% yield.
  • 11
    • 33750952305 scopus 로고    scopus 로고
    • note
    • 2 = 0.0812 [I > 2σ(I)]. Structural measurements were both performed on a Bruker SMART 1000 CCD diffractometer equipped with graphite-monochromated Mo Kα radiation with radiation wavelength 0.71073 Å by using the ω-φ{symbol} scan technique. The structures were solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 programs [13]. CCDC Nos. 261123 (1) and 196146 (2) contain the supplementary crystallographic data. These data can be obtained via the Cambridge Crystallographic Data Centre. Available from: , .
  • 12
    • 33750937233 scopus 로고    scopus 로고
    • note
    • 6Cu: found: C, 45.20; H, 3.77; N, 17.55. Calc.: C, 45.23; H, 3.80; N, 17.58.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.