Synthesis of titanium oxide particles in supercritical CO2: Effect of operational variables in the characteristics of the final product

Journal of Supercritical Fluids

Volumn 39, Issue 3, 2007, Pages 453-461

  Alonso, E ^a   Montequi, I ^a   Lucas, S ^a   Cocero, M J ^a  

^a UNIVERSITY OF VALLADOLID   (Spain)

Author keywords

Particle synthesis; Supercritical synthesis; TiO2

Indexed keywords

CARBON DIOXIDE; CRYSTAL GROWTH; HYDROLYSIS; NANOSTRUCTURED MATERIALS; ORGANOMETALLICS; PARTICLE SIZE ANALYSIS; REACTION KINETICS; SUPERCRITICAL FLUIDS; SYNTHESIS (CHEMICAL);

METAL CLUSTERS; PARTICLE SYNTHESIS; SUPERCRITICAL SYNTHESIS; TITANIUM TETRAISOPROPOXIDE (TTIP);

TITANIUM OXIDES;

EID: 33750743802     PISSN: 08968446     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.supflu.2006.03.006     Document Type: Article

References (24)

1. Adschiri T. Applications of supercritical fluids in powder processing. KONA Powder Part. 16 (1998) 89
2. Teja A.S., and Holm L.J. Production of magnetic nanoparticles using supercritical fluids. In: Sun Y.-P. (Ed). Supercritical Fluid Technology in Materials Science and Engineering (2002), Marcel Dekker Inc. 0-82-470651-X 311
3. Blackburn J.M., Long D.P., Cabañas A., and Watkins J.J. Deposition of conformal copper and nickel films from supercritical carbon dioxide. Science 294 (2001) 141
4. 2 membranes using supercritical alcohols. Mater. Chem. Phys. 64 (2000) 156
5. M'Hamdi R., Bouquet J.F., Chhor K., and Pommier C. Solubility decomposition studies on metal chelates in supercritical fluids for ceramic precursors powders synthesis. J. Supercrit. Fluids 4 (1991) 55
6. Adschiri T., and Arai K. Hydrothermal synthesis of metal oxide nanoparticles under supercritical conditions. In: Sun Y.-P. (Ed). Supercritical Fluid Technology in Materials Science and Engineering (2002), Marcel Dekker Inc. 0-82-470651-X 311
7. 2 using fluorinated ligands. J. Am. Chem. Soc. 122 (2000) 4245
8. Johnston K.P., et al. Microemulsions, emulsions and latexes. In: Jessu J. (Ed). Chemical Synthesis Supercritical Fluids (1999), John Wiley and Sons, New York 127
9. Jung J., and Perrut M. Particle design using supercritical fluids: literature and patent survey. J. Supercrit. Fluids 20 (2001) 179
10. Sun Y.-P. Supercritical Fluid Technology in Materials Science and Engineering (2001), Marcel Dekker Inc. 0-82-470651-X
11. Cansell F., Aymonier C., and Loppinet-Serani A. Review on materials science and supercritical fluids. Curr. Opin. Solid State Mater. Sci. 7 4-5 (2003) 331
12. Diebold U. The surface science of titanium dioxide. Surf. Sci. Rep. 48 (2003) 53
13. 2. J. Supercrit. Fluids 9 (1996) 172
14. 2 powders in vapor, liquid and supercritical phases: a comparative study. Mater. Chem. Phys. 32 (1992) 249
15. Gourinchas V., Chhor K., Bocquet J.F., and Pommier C. Kinetics of the titanium isopropoxide decomposition in supercritical isopropyl alcohol. Ind. Eng. Chem. Res. 35 (1996) 2539
16. Adschiri T., Hakuta Y., and Arai K. Hydrothermal synthesis of metal oxide fine particles at supercritical conditions. Ind. Eng. Chem. Res. 39 (2000) 4901
17. Reverchon E., Caputo G., Correra S., and Cesti P. Synthesis of titanium hydroxide nanoparticles in supercritical carbon dioxide on the pilot scale. J. Supercrit. Fluids 26 (2003) 253
18. Papet S., Sarrade S., Julbe A., and Guizard C. Titanium hydroxide synthesis in supercritical solvent. In: Poliakoff M., George M.W., and Howdle S.M. (Eds). Proceedings of the 6th Meeting on Supercritical Fluids, Chemistry and Materials. Nottingham, April 10-13 (1999). 2-905-267-30-5 17
19. Cansell F., Chevalier B., Demourgues A., Etourneau J., Even C., Garrabos Y., Pessey V., Petit S., Tressaud A., and Weill F. Supercritical fluid processing: a new route for material synthesis. J. Mater. Chem. 9 (1999) 67
20. 2 + saturated alcohol. J. Supercrit. Fluids 20 (2001) 229
21. Martín A., and Cocero M.J. Numerical modelling of jet hydrodynamics, mass transfer, and crystallization kinetics in the supercritical antisolvent (SAS) process. J. Supercrit. Fluids 32 (2004) 203
22. 2/ethanol mixtures. J. Mater. Chem. 12 4 (2002) 958
23. Buining P.A., Pathmamanoharan C., Bosboom M., Jansen J.B.H., and Lekerkerker H.N.W. Effect of hydrothermal conditions on the morphology of colloidal Boehmite particles: implication for fibril formation and monodispersity. J. Am. Ceram. Soc. 73 8 (1990) 2185
24. 2 fine crystals for lithium batteries by hydrothermal synthesis under supercritical condition. High Pressure Res. 20 1-6 (2001) 373