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21
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33750698029
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note
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III-OOR species during the manual mixing time in the EPR tube. In contrast, the UV-vis spectra for 2 are obtained within a few seconds after addition of ROOH. Moreover, the ∼5-fold increase in concentration of reactants in the EPR experiments compared to those used in the UV-vis will accelerate intermolecular decay pathways. Thus, it is reasonable to estimate e values for 2 based on 100% conversion despite the EPR quantitation measurements.
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22
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33750733693
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note
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Deuteration of 1 at the N-H positions does not change the v(Fe-O), ruling out hydrogen bonding as the cause of the low frequency.
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