Improving and speeding up the characterization of substances, materials, and products: Benefits and potentials of high-speed DSC

American Laboratory

Volumn 38, Issue 14, 2006, Pages 21-25

  Mathot, Vincent B F ^a,b   Vanden Poel, Geert ^c   Pijpers, Thijs F J ^b  

^a SciTe BV   (Netherlands)

^b UNIVERSITY OF LEUVEN   (Belgium)

^c DSM RESOLVE   (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

COCRYSTALLIZATION; MOLAR MASSES; SHORT CHAIN BRANCHES (SCB);

CRYSTALLIZATION; DRUG PRODUCTS; HEAT FLUX; POLYMERS; SIZE EXCLUSION CHROMATOGRAPHY;

DIFFERENTIAL SCANNING CALORIMETRY;

EID: 33750435214     PISSN: 00447749     EISSN: None     Source Type: Trade Journal    
DOI: None     Document Type: Article

References (8)

1. Pijpers, T.F.J.; Mathot, V.B.F.; Goderis, B.; Scherrenberg, R.L.; van der Vegte, E.W. High-speed calorimetry for the study of the kinetics of (de)vitrification, crystallization, and melting of macromolecules. Macromolecules 2002, 35, 3601-13.
2. Vanden Poel, G.; Mathot, V.B.F. High speed/high performance differential scanning calorimetry (HPer DSC): temperature calibration in the heating and cooling mode and minimization of thermal lag. Thermochim. Acta, available on-line Mar 6, 2006, doi:10.1016/j.tca.2006.02.022.
3. Efremov, M.Y.; Warren, J.T.; Olson, E.A.; Zhang, M.; Kwan, A.T.; Allen, L.H. Thin-film differential scanning calorimetry: a new probe for assignment of the glass transition of ultrathin polymer films. Macromolecules 2002, 35(5), 1481-3.
4. Tol, R.T.; Minakov, A.A.; Adamovsky, S.A.; Mathot, V.B.F.; Schick, C. Metastability of polymer crystallites formed at low temperature studied by ultra fast calorimetry: polyamide 6 confined in sub-micrometer droplets vs. bulk PA6. Polymer 2006, 47, 2172-8.
5. Herwaarden, A.W. Overview of calorimeter chips for various applications. Thermochim. Acta 2005, 432(2), 192-201.
6. Gabbott, P.; Clarke, P.; Mann, T.; Royall, P.; Shergill, A. A high-sensitivity, high-speed DSC technique: measurement of amorphous lactose. Am. Lab. 2003, 35(16), 17-22.
7. www.hyperdsc.com; see also webcast by V. Mathot through this Web site; www.scite.nl.
8. Luruli, N.; Pijpers, T.; Brüll, R.; Grumel, V.; Pasch, H.; Mathot, V.B.F. Submitted, J. Polym. Sci. Part B: Polym. Phys.