-
2
-
-
8644275496
-
-
references cited therein
-
Non-aqueous methods for ester hydrolysis have been reported. For example, see: Anderson, M. O.; Moser, J.; Sherrill, J.; Guy, R. K. Synlett 2004, 2391 and references cited therein.
-
(2004)
Synlett
, vol.2391
-
-
Anderson, M.O.1
Moser, J.2
Sherrill, J.3
Guy, R.K.4
-
3
-
-
20844433475
-
-
(a) Ley, S. V.; Baxendale, I. R.; Bream, R. N.; Jackson, P. S.; Leach, A. G.; Longbottom, D. A.; Nesi, M.; Scott, J. S.; Storer, R. I.; Taylor, S. J. J. Chem. Soc., Perkin Trans. I 2000, 3815.
-
(2000)
J. Chem. Soc., Perkin Trans. I
, pp. 3815
-
-
Ley, S.V.1
Baxendale, I.R.2
Bream, R.N.3
Jackson, P.S.4
Leach, A.G.5
Longbottom, D.A.6
Nesi, M.7
Scott, J.S.8
Storer, R.I.9
Taylor, S.J.10
-
4
-
-
0033052277
-
-
(b) Drewry, D. H.; Coe, D. M.; Poon, S. Med. Res. Rev. 1999, 19, 97.
-
(1999)
Med. Res. Rev.
, vol.19
, pp. 97
-
-
Drewry, D.H.1
Coe, D.M.2
Poon, S.3
-
6
-
-
33750053184
-
Polymer-supported hydroxide
-
Wipf, P. Ed.; Handbook of Reagents for Organic Synthesis Series; John Wiley & Sons: The Atrium, Southern Gate, Chichester, West Sussex PO19 8SQ, England
-
(a) Ley, S. V.; Baxendale, I. R.; Le, A-L. Polymer-supported Hydroxide. In Reagents for High-Throughput Solid-Phase and Solution-Phase Organic Synthesis; Wipf, P. Ed.; Handbook of Reagents for Organic Synthesis Series; John Wiley & Sons: The Atrium, Southern Gate, Chichester, West Sussex PO19 8SQ, England, 2005; p 235.
-
(2005)
Reagents for High-Throughput Solid-Phase and Solution-Phase Organic Synthesis
, pp. 235
-
-
Ley, S.V.1
Baxendale, I.R.2
Le, A.-L.3
-
7
-
-
0021703205
-
-
(b) Cardillo, G.; Orena, M; Sandri, S.; Tomasini, C. J. Org. Chem. 1984, 49, 3951.
-
(1984)
J. Org. Chem.
, vol.49
, pp. 3951
-
-
Cardillo, G.1
Orena, M.2
Sandri, S.3
Tomasini, C.4
-
8
-
-
37049126451
-
-
Arcus, C. L.; Gonzalez, C. G.; Linnecar, D. F. C. J. Chem. Soc. Chem. Commun. 1969, 23, 1377.
-
(1969)
J. Chem. Soc. Chem. Commun.
, vol.23
, pp. 1377
-
-
Arcus, C.L.1
Gonzalez, C.G.2
Linnecar, D.F.C.3
-
9
-
-
0037025957
-
-
(d) Baxendale, I. R.; Ley, S. V.; Nessi, M.; Piutti, C. Tetrahedron 2002, 58, 6285.
-
(2002)
Tetrahedron
, vol.58
, pp. 6285
-
-
Baxendale, I.R.1
Ley, S.V.2
Nessi, M.3
Piutti, C.4
-
10
-
-
0034040896
-
-
(a) South, M. S.; Case, B. L.; Dice, T. A.; Franklin, G. W.; Hayes, M. J.; Jones, D. E.; Lindmark, R. J.; Zeng, Q.; Parlow, J. J. Comb. Chem. High Throughput Screening 2000, 3, 139.
-
(2000)
Comb. Chem. High Throughput Screening
, vol.3
, pp. 139
-
-
South, M.S.1
Case, B.L.2
Dice, T.A.3
Franklin, G.W.4
Hayes, M.J.5
Jones, D.E.6
Lindmark, R.J.7
Zeng, Q.8
Parlow, J.J.9
-
11
-
-
0035847455
-
-
(b) Hardcastle, I. R.; Barber, A. M.; Marriott, J. H.; Jannan, M. Tetrahedron Lett. 2001, 42, 1363.
-
(2001)
Tetrahedron Lett.
, vol.42
, pp. 1363
-
-
Hardcastle, I.R.1
Barber, A.M.2
Marriott, J.H.3
Jannan, M.4
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13
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33750083527
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note
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The choice of methanol was based on the observation that all the commercially available acid products had good solubility in this solvent.
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14
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0020719564
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-
Kim, B.; Kirszensztejn, P.; Bolikal, D.; Regen, S. L. J. Am. Chem. Soc. 1983, 105, 1567.
-
(1983)
J. Am. Chem. Soc.
, vol.105
, pp. 1567
-
-
Kim, B.1
Kirszensztejn, P.2
Bolikal, D.3
Regen, S.L.4
-
15
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0001503468
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-
Bobbitt, J. M.; Scola, D. A. J. Org. Chem. 1960, 25, 560. It is noteworthy that although some hydrolysis of the aromatic nitrile was observed under the reaction conditions, for the reactions run in acetonitrile, no hydrolysis of the solvent aliphatic nitrile was observed.
-
(1960)
J. Org. Chem.
, vol.25
, pp. 560
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-
Bobbitt, J.M.1
Scola, D.A.2
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16
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0003767657
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Appendix D.
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Blevins, D. D.; Burke, M. F.; Good, T. J.; Harris, P. A.; Van Horne, K. C.; Simpson, N.; Yago, L. S. Appendix D. In Sorbent Extraction Technology, 2nd ed.;
-
Sorbent Extraction Technology, 2nd Ed.
-
-
Blevins, D.D.1
Burke, M.F.2
Good, T.J.3
Harris, P.A.4
Van Horne, K.C.5
Simpson, N.6
Yago, L.S.7
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17
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33750092155
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-
Simpson, N., Van Horne, K. C., Eds.; Varian Sample Preparation Products: Harbor City, CA
-
Simpson, N., Van Horne, K. C., Eds.; Varian Sample Preparation Products: Harbor City, CA, 1993; pp 118-120.
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(1993)
, pp. 118-120
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18
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33750049552
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note
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It was observed that dilute HCl could not be used in methanol because re-esterification of product acids was noted. Formic acid did not demonstrate this liability for the examples described herein.
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