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33750056571
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note
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Optical purity of 5-phenyl dihydrofuran was 88% ee.
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25
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33750076553
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note
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3, Z = 4; Mo Kα radiation (λ = 0.71073 Å, T = 150 K), R1 = 0.045, wR2 = 0.076 (I > 2σ(I)); R1 = 0.081, wR2 = 0.089 (all data). Crystallographic data has been deposited with the Cambridge Crystallographic Data Center (deposition no. 611303). These data can be obtained free of charge via the Internet at www.ccdc.cam.ac.uk/data_request/cif, by email to data_request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, U.K.
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