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2NH group, has also been studied recently. For a review of Salan complexes of the Group 12, 13, and 14 elements, see: D. A. Atwood, Coord. Chem. Rev., 1997, 165, 267.
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But,Me]AlR (R = Me, Et), have been prepared. See: I. Taden, H.-C. Kang, W. Massa and J. Okuda, J. Organomet. Chem., 1997, 540, 189.
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84970610691
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This method has previously been used for the synthesis of [Salen]Sn and related complexes. See: A. M. van den Bergen, J. D. Cashion, G. D. Fallon and B. O. West, Aust. J. Chem., 1990, 43, 1559.
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33748969239
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[Saldph] differs from [Salen] in being derived from 4,5-dimethylphenylene-1,2-diamine rather than ethylenediamine
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[Saldph] differs from [Salen] in being derived from 4,5-dimethylphenylene-1,2-diamine rather than ethylenediamine.
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22
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0001946975
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2 are, however, known. See, for example: (a) J. Parr, A. T. Ross and A. M. Z. Slawin, J. Chem. Soc., Dalton Trans., 1996, 1509;
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2] coordination core is planar and the ligand adopts an approximately planar geometry, see: A. G. Manfredotti and C. Guastini, Acta Crystallogr., Sect. C, 1983, 39, 863.
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33748954511
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note
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2] mirror plane (see Fig. 2 and 3). If the bridge is sufficiently flexible that a planar arrangement may be obtained, the spin system simplifies to AA′BB′.
-
-
-
-
34
-
-
33748984318
-
-
note
-
207Pb-H) coupling at high temperatures suggests that dissociation of lead is not involved and that the exchange is intramolecular.
-
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-
-
35
-
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33748953603
-
-
note
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-
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-
-
36
-
-
33748977170
-
-
note
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117Sn)= 1.05, due to the ratio of the respective magnetogyric ratios. See ref. 21.
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