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Alternatively, compounds 2-5 can also be prepared by the addition of the respective substituted pyridine ligand to a methanol solution of 1. By this route, better yields and good-quality crystals are obtained.
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28
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33748651363
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2 = 0.0705, GOF = 0.907. CCDC-289557 (3), -289558 (4), -289559 (2), and -289560 (5) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_ request/cif.
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