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note
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2).
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12
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33748270042
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note
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3). This compound is very sensitive to air.
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13
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33748272314
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note
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-1, R1 = 0.0469, wR2 = 0.1300. Data were collected on a Bruker SMART automatic diffractometer using graphite-monochromated Mo Kα (λ = 0.710 73 Å) radiation. Structures were solved by direct methods (SIR-2004) and refined by full-matrix least-squares refinement using the SHELXL97 program.
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15
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19
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33748283740
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note
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The data were corrected for diamagnetic contributions and included for temperature-independent paramagnetism.
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20
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33751499295
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