Active sampling followed by solid-phase microextraction for the determination of pyrethroids in indoor air

Journal of Chromatographic Science

Volumn 44, Issue 7, 2006, Pages 430-437

  Barro, Ruth ^a   Garcia Jares, Carmen ^a   Llompart, Maria ^a   Cela, Rafael ^a  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33746931721     PISSN: 00219665     EISSN: 00219665     Source Type: Journal    
DOI: 10.1093/chromsci/44.7.430     Document Type: Article

References (24)

1. J.R. Reigart and J.R. Roberts. Recognition and Management of Pesticide Poisonings, 5th ed. U.S. Environment Protection Agency, Washington, D.C., 1999.
2. Agency for Toxic Substances and Disease Registry (ATSDR). Toxicological Profile for Pyrethrins and Pyrethroids. U.S. Department of Health and Human Services, Public Health Service, Atlanta, GA, 2003.
3. L. Elflein, E. Berger-Preiss, K. Levsen, and G. Wünsch. Development of a gas chromatography-mass spectrometry method for the determination of household insecticides in indoor air. J. Chromatogr. A 985: 147-57 (2003).
4. T. Yoshida, I. Matsunaga, and H. Oda. Simultaneous determination of semivolatile organic compounds in indoor air by gas chromatography-mass spectrometry after solid-phase extraction. J. Chromatogr. A 1023: 255-69 (2004).
5. R.P. Miskus and T.L. Andrews. Stabilization of thin films of pyrethrins and allethrin. J. Agr. Food Chem. 20: 313-15 (1972).
6. J. Pawliszyn. Solid-Phase Microextraction: Theory and Practice. Wiley-VCH, New York, NY, 1997.
7. J.A. Koziel and I. Novak. Sampling and sample-preparation strategies based on solid-phase microextraction for analysis of indoors air. Trends Anal. Chem. 21: 840-50 (2002).
8. J. Beltran, A. Peruga, E. Pitarch, F.J. López, and F. Hernández. Application of solid-phase microextraction for the determination of pyrethroid residues in vegetable samples by GC-MS. Anal. Bioanal. Chem. 376: 502-11 (2003).
9. W. Liu and J.J. Gan. Separation and analysis of diastereomers and enantiomers of cypermethrin and cyfluthrin by gas chromatography. J. Agric. Food Chem. 52: 736-41 (2004).
10. W.R. Barrionuevo and F.M. Lanças. Solid-phase microextraction of pyrethroid pesticides from water at low and sub-ppt levels at different temperatures. J. High Resolut. Chromatogr. 23: 485-88 (2000).
11. W.R. Barrionuevo and F.M. Lanças. Comparison of liquid-liquid extraction (LLE), solid-phase extraction (SPE), and solid-phase microextraction (SPME) for pyrethroid pesticides analysis from enriched river water. Bull. Environ. Contam. Toxicol. 69: 123-28 (2002).
12. C. Gonçalves and M.F. Alpendurada. Comparison of three different poly(dimethylsiloxane)-divinylbenzene fibres for the analysis of pesticide multiresidues in water samples: structure and efficiency. J. Chromatogr. A 963: 19-26 (2002).
13. C. Gonçalves and M.F. Alpendurada. Multiresidue method for the simultaneous determination of four groups of pesticides in ground and drinking waters, using solid-phase microextraction-gas chromatography with electron-capture and thermionic specific detection. J. Chromatogr. A 968: 177-90 (2002).
14. A. Sanusi, V. Guillet, and M. Montury. Advanced method using microwaves and solid-phase microextraction coupled with gas chromatography-mass spectrometry for the determination of pyrethroid residues in strawberries. J. Chromatogr. A 1046: 35-40 (2004).
15. F. Ferrari, A. Sanusi, M. Millet, and M. Montury. Multiresidue method using SPME for the determination of various pesticides with different volatility in confined atmospheres. Anal. Bioanal. Chem. 379: 476-83 (2004).
16. A. Saba, A. Cuzzola, A. Raffaelli, S. Pucci, and P. Salvadori. A simple method for the extraction of volatile organic compounds contained in air samples from adsorbent materials by solid phase microextraction and their analysis by gas chromatography/mass spectrometry. Rapid Commun. Mass Spectrom. 13: 1899-1902 (1999).
17. A. Saba, A. Cuzzola, A. Raffaelli, S. Pucci, and P. Salvadori. Determination of benzene at trace levels in air by a novel method based on solid-phase microextraction gas chromatography/mass spectrometry. Rapid Commun. Mass Spectrom. 15: 2404-2408 (2001).
18. R. Barro, S. Ares, C. Garcia-Jares, M. Llompart, and R. Cela. Development of a sensitive methodology for the analysis of chlorobenzenes in air by combination of solid-phase extraction and headspace solid-phase microextraction. J. Chromatogr. A 1045: 189-96 (2004).
19. R. Barro, S. Ares, C. Garcia-Jares, M. Llompart, and R. Cela. Sampling and analysis of polychlorinated biphenyls in indoor air by sorbent enrichment followed by headspace solid-phase microextraction and gas chromatography-tandem mass spectrometry. J. Chromatogr. A 1072: 99-106 (2005).
20. M. Harper. Sorbent trapping of volatile organic compounds from air. J. Chromatogr. A 885: 129-51 (2000).
21. J. You, D.P. Weston, and M.J. Lydy. A sonication extraction method for the analysis of pyrethroid, organophosphate, and organochlorine pesticides from sediment by gas chromatography with electron-capture detection. Arch. Environ. Contam. Toxicol. 47: 141-47 (2004).
22. Statgraphics-Plus. "Appendix C". In Experimental Design. Manugistics Inc., Rockville, Maryland, 2002.
23. A. Ramesh and A. Vijayalakshmi. Monitoring of allethrin, deltamethrin, esbiothrin, prallethrin and transfluthrin in air during the use of household mosquito repellents. J. Environ. Monit. 3: 191-93 (2001).
24. S. Oepkemeier, S. Schreiber, D. Breuer, G. Key, and W. Kleiböhmer. Determination of permethrin in indoor air by liquid chromatography with enzyme linked immunosorbent assay. Anal. Chim. Acta 393: 103-108 (1999).