Microwave-assisted synthesis of (η6-arene)tricarbonylchromium complexes

Tetrahedron Letters

Volumn 47, Issue 37, 2006, Pages 6569-6572

  Lee, Young Tak ^a   Choi, Soo Young ^a   Lee, Sang Ick ^a   Chung, Young Keun ^a   Kang, Tae Jin ^b  

^a Seoul National University   (South Korea)

^b Seoul National University   (South Korea)

Author keywords

[No Author keywords available]

Indexed keywords

CHROMIUM DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL REACTION; COMPLEX FORMATION; MICROWAVE RADIATION; REACTION ANALYSIS; SYNTHESIS;

EID: 33746799287     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.07.011     Document Type: Article

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40. 2 solution. (1m) Crystal data: crystal system, monoclinic, P21/n, unit cell dimensions, a = 7.6094(5) Å, b = 15.2373(10) Å, c = 13.5676(9) Å, α = 90°, β = 104.6800(10)°, γ = 90°. Final R indices [I > 2sigma(I)], R1 = 0.0650, wR2 = 0.1212. CCDC reference number: 611497. (1n) Crystal data: crystal system, monoclinic, P21/n, unit cell dimensions, a = 11.7535(8) Å, b = 12.6540(10) Å, c = 15.1559(10) Å, α = 90°, β = 94.756(2)°, γ = 90°. Final R indices [I > 2sigma(I)], R1 = 0.0538, wR2 = 0.368. CCDC reference number: 611498.