Characterization of the bis-silylated endofullerene Sc3N@C 80

Journal of the American Chemical Society

Volumn 128, Issue 30, 2006, Pages 9919-9925

  Wakahara, Takatsugu ^a   Iiduka, Yuko ^a   Ikenaga, Ozora ^a   Nakahodo, Tsukasa ^a   Sakuraba, Akihiro ^b   Tsuchiya, Takahiro ^a   Maeda, Yutaka ^c   Kako, Masahiro ^d   Akasaka, Takeshi ^a   Yoza, Kenji ^e   Horn, Ernst ^f   Mizorogi, Naomi ^g   Nagase, Shigeru ^g  

^a UNIVERSITY OF TSUKUBA   (Japan)

^b NIIGATA UNIVERSITY   (Japan)

^c TOKYO GAKUGEI UNIVERSITY   (Japan)

^d UNIVERSITY OF ELECTRO COMMUNICATIONS   (Japan)

^e BRUKER AXS INC   (United States)

^f RIKKYO UNIVERSITY   (Japan)

^g INSTITUTE FOR MOLECULAR SCIENCE   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC COMPOUNDS; PHOTOCHEMICAL REACTIONS; PROBABILITY DENSITY FUNCTION; SINGLE CRYSTALS; X RAY ANALYSIS;

1,1,2,2-TETRAMESITYL-1,2-DISILIRANE; BIS-SILYLATED ENDOFULLERENE; X-RAY STRUCTURE ANALYSIS;

SCANDIUM COMPOUNDS;

FULLERENE DERIVATIVE; SILICON DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; CRYSTAL STRUCTURE; DENSITY FUNCTIONAL THEORY; INFRARED SPECTROSCOPY; ISOMER; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OXIDATION REDUCTION REACTION; PHOTOCHEMISTRY; SILYLATION; STRUCTURE ANALYSIS; X RAY CRYSTALLOGRAPHY;

EID: 33746621286     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja062233h     Document Type: Article

References (33)

1. Heath, J. R.; O'Brien, S. C.; Liu, Y.; Curl, R. F.; Kroto, H. W.; Title, F. K.; Smalley, R. E. J. Am. Chem. Soc. 1985, 107, 7779-7780.
2. Chai, Y.; Guo, T.; Jin, C.; Haufler, R. E.; Chibante, L. P. F.; Fure, J.; Wang, L.; Alford, J. M.; Smalley, R. E. J. Phys. Chem. 1991, 95, 7564-7568.
3. Endofullerenes: A New Family of Carbon Clusters; Akasaka, T., Nagase, S., Eds.; Kluwer: Dordrecht, The Netherlands, 2002.
4. Stevenson, S.; Rice, G.; Glass, T.; Harich, K.; Cromer, F.; Jordan, M. R.; Craft, J.; Hadju, E.; Bible, R.; Olmstead, M. M.; Maitra, K.; Fisher, A. J.; Balch, A. L. Dorn, H. C. Nature 1999, 401, 55-57.
5. Krätschmer, W.; Lamb, L. D.; Fostiropoulus, K.; Huffman, D. R. Nature 1990, 347, 354-358.
6. Kobayashi, K.; Sano, Y.; Nagase, S. J. Comput. Chem. 2001, 13, 1353-1358.
7. (b) Campanera, J. M.; Bo, C.; Olmstead, M. M.; Balch, A. L.; Poblet, J. M. J. Phys. Chem. A 2002, 106, 12356-12364.
8. Lee, H. M.; Olmstead, M. M.; Iezzi, E.; Duchamp, J. C.; Dorn, H. C.; Balch, A. L. J. Am. Chem. Soc. 2002, 124, 3494-3495.
9. (b) Maeda, Y.; et al. J. Am. Chem. Soc. 2004, 126, 6858-6859.
10. (c) Cardona, C. M.; Kitaygorodskiy, A.; Ortiz, A.; Herranz, M. A.; Echegoyen, L. J. Org. Chem. 2005, 70, 5092-5097.
11. (d) Cao, B.; Wakahara, T.; Maeda, Y.; Han, A. Akasaka, T.; Kato, T.; Kobayashi, K.; Nagase, S. Chem.-Eur. J. 2004, 10, 716-720.
12. (e) Kareev, I. E.; Lebedkin, S. F.; Bubnov, V. P.; Yagubskii, E. B.; Ioffe, I. N.; Khavre, P. A.; Kuvychko, I. V.; Strauss, S. H.; Boltalina, O. V. Angew, Chem. Int. Ed. 2005, 44, 2-5.
13. The Chemistry of Organic Silicon Compounds; Patai, S., Rappoport, Z., Eds.; Wiley: Chichester, U.K., 1989.
14. Wakahara, T.; Maeda, Y.; Kako, M.; Akasaka, T.; Kobayashi, K.; Nagase, S. J. Organomet. Chem. 2003, 685, 177-188.
15. (b) Wakahara, T.; Kako, M.; Maeda, Y.; Akasaka, T.; Kobayashi, K.; Nagase, S. Curr. Org. Chem. 2003, 7, 927-943.
16. Ando, W.; Kako, M.; Akasaka, T.; Nagase, S. Organometallics 1993, 12, 1514-1522 and references therein.
17. (b) Masamune, S.; Murakami, S.; Tobita, H.; Williams, D. J. J. Am. Chem. Soc. 1983, 105, 7776-7778.
18. Akasaka, T.; Kato, T.; Kobayashi, K.; Nagase, S.; Yamamoto, K.; Funasaka, H.; Takahashi, T. Nature 1995, 374, 600-601.
19. (b) Wakahara, T.; Kobayashi, J.; Yamada, M.; Maeda, Y.; Tsuchiya, T.; Okamura, M.; Akasaka, T.; Waelchli, M.; Kobayashi, K.; Nagase, S.; Kato, T.; Kako, M.; Yamamoto, K.; Kadish, K. M. J. Am. Chem. Soc. 2004, 126, 4883-4887.
20. (c) Akasaka, T.; Okubo, S.; Kondo, M.; Maeda, Y.; Wakahara, T.; Kato, T.; Suzuki, T.; Yamamoto, K.; Kobayashi, K.; Nagase, S. Chem. Phys. Lett. 2000, 319, 153-156.
21. (d) Akasaka, T.; Nagase, S.; Kobayashi, K.; Suzuki, T.; Kato, T.; Yamamoto, K.; Funasaka, H.; Takahashi, T. J. Chem. Soc., Chem. Commun. 1995, 1343-1344.
22. (e) Akasaka, T.; Nagase, S.; Kobayashi, K.; Suzuki, T.; Kato, T.; Kikuchi, K.; Achiba, Y.; Yamamoto, K.; Funasaka, H.; Takahashi, T. Angew. Chem., Int. Ed. Engl. 1995, 34, 2139-2141.
23. (f) Wakahara, T.; Sakuraba, A.; Iiduka, Y.; Okamura, M.; Tsuchiya, T.; Maeda, Y.; Ishizuka, M. O.; Akasaka, T.; Okubo, S.; Kato, T.; Kobayashi, K.; Nagase, S.; Kadish, K. M. Chem. Phys. Lett. 2004, 398, 553-555.
24. (g) Yamada, M.; Feng, L.; Wakahara, T.; Tsuchiya, T.; Maeda, Y.; Lian, Y.; Kako, M.: Akasaka, T.; Kato, T.; Kobayashi, K.; Nagase, S. J. Phys. Chem. B 2005, 109, 6049-6051.
25. (h) Yamada, M.; Nakahodo, T.; Wakahara, T.; Tsuchiya, T.; Maeda, Y.; Akasaka, T.; Kako, M.; Yoza, K.; Horn, E.; Mizorogi, N.; Kobayashi, K.; Nagase, S. J. Am. Chem. Soc. 2005, 127, 14570-14571.
26. Iiduka, Y.; Ikenaga, O.; Sakuraba, A.; Wakahara, T.; Tsuchiya, T.; Maeda, Y.; Nakahodo, T.; Akasaka, T.; Kako, M.; Mizorogi, N.; Nagase, S. J. Am. Chem. Soc. 2005, 127, 9956-9957.
27. Becke, A. D. Phys. Rev. A 1988, 38, 3098-3100.
28. Becke, A. D. J. Chem. Phys. 1993, 98, 5648-5652.
29. Lee, C.; Yang, W.; Parr, R. G. Phys. Rev. B 1988, 37, 785-789.
30. Frisch, M. J.; et al. GAUSSIAN 03, revision C. 01; Gaussian Inc.: Wallingford, CT, 2004.
31. Hay, P. J.; Wadt, W. R. J. Chem. Phys. 1985, 82, 299-310.
32. Hehre, W. J.; Ditchfield, R.; Pople, J. A. J. Chem. Phys. 1972, 56, 2257-2261.
33. Akasaka, T.; et al. Org. Lett. 2000, 2, 2671-2674.