Photochemical reaction of Mo(CO)6 with et2SiH 2: Spectroscopic characterization and crystal structure of the Bis{(μ-η2-hydridodiethylsilyl)tetracarbonylmolybdenum(I)} complex [{Mo(μ-η2-H-SiEt2)(CO)4} 2]

Organometallics

Volumn 25, Issue 15, 2006, Pages 3791-3794

  Stosur, Magdalena ^a   Kochel, Andrzej ^a   Keller, Antoni ^a   Szymańska Buzar, Teresa ^a  

^a UNIVERSITY OF WROC AW   (Poland)

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL BONDS; CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANOMETALLICS; PHOTOCHEMICAL REACTIONS; PHOTOLYSIS; SPECTROSCOPIC ANALYSIS; SPECTRUM ANALYSIS;

HIGH-FIELD RESONANCE; MOLYBDENUM HYDRIDES; NMR SPECTRUM; QUINTETS;

MOLYBDENUM COMPOUNDS;

EID: 33746368691     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om060290d     Document Type: Article

References (43)

1. (a) schroeder, M. A.; wrigmon, M. s. J. Am. Chem. soc. 1974, 96, 6235.
2. (b) Abdelgader, W.; Chmielewski, D.; Grevels, F.-W.; Özkar, S.; Peynircioglu, N. B. Organometallics 1996, 15, 604.
3. (c) Brunner, H.; Weber, M.; Zabel, M. J. Organomet. Chem. 2003, 684, 6.
4. (d) Ganicz, T.; Mizerska, U.; Moszner, M.; O'Brien, M.; Perry, R.; Stańczyk, W. A. Appl. Catal. Gen. 2003, 259, 49.
5. (e) Gustafsson, M.; Frejd, T. J. Organomet. Chem. 2004, 689, 438.
6. (f) Arena, C. G.; Pattacini, R. J. Mol. Catal. A; Chem. 2004, 222, 47.
7. (g) Paris, S. I. M.; Lemke, F. R. Inorg. Chem. Commun. 2005, 8, 425.
8. (h) Imilinger, N.; Wurst, K.; Buchmeiser, M. R. J. Organomet. Chem. 2005, 690, 4433.
9. Barieille, L.; Becht, S.; Cui, J. L.; Gendre, P.; Moïse, C. Organometallics 2005, 24, 5802.
10. (j) Marciniec, B. Coord. Chem. Rev. 2005, 249, 2374.
11. (a) Elder, M. Inorg. Chem. 1970, 9, 762.
12. (b) Bennett, M. J.; Simpson, K. A. J. Am. Chem. Soc. 1971, 93, 7156.
13. (c) Kawano, Y.; Tobita, H.; Ogino, H. J. Organomet. Chem. 1992, 428, 125.
14. (d) Luo, X.-L.; Kubas, G. J.; Bryan, J. C.; Bums, C. J.; Unkefer, C. J. J. Am. Chem. Soc. 1994, 116, 10312.
15. (e) Luo, X.-L.J Kubas, G. J.; Burns, C. J.; Bryan, J. C.; Unkefer, C. J. J. Am. Chem. Soc. 1995, 177, 1159.
16. (f) Simons, R. S.; Tessier, C. A. Organometallics 1996, 15, 2604.
17. (g) Butts, M. D.; Bryan, J. C. Luo, X.-L.; Kubas, G. J. Inorg. Chem. 1997, 36, 3341.
18. (h) Corey, J. Y.; Braddock-Wiking, J. Chem. Rev. 1999, 99, 175.
19. Lin, Z. Chem. Soc. Rev. 2002, 31, 239.
20. (j) Yu, X.; Morton, L. A.; Xue, Z.-L. Organometallics 2004, 32, 2210.
21. Ga̧dek, A.; Kochel, A.; Szymańska-Buzar, T. Organometallics 2003, 22, 4869.
22. (a) Darensbourg, M. Y.; Slater, S. J. Am. Chem. Soc. 1981, 103, 5914.
23. (b) Lin, J. T.; Hagen, G. P.; Ellis, J. E. J. Am. Chem. Soc. 1983, 105, 2296.
24. (c) Hayter, R. G. J. Am. Chem. Soc. 1966, 88, 4376.
25. (d) Petersen, J. L.; Masino, A.; Stewart, R. P. J. Organomet. Chem. 1981, 208, 55.
26. (e) Lin, T. J.; Ellis, J. E. J. Am. Chem. Soc. 1983, 105, 6252.
27. (a) Koloski, T. S.; Pestana, D. C.; Carroll, P. J.; Berry, D. H. Organometallics 1994, 13, 489.
28. (b) Mork, B. V.; Tilley, T. D. Angew. Chem., Int. Ed. 2003, 42, 357.
29. (a) Jaitner, P.; Wohlgenannt, W. Montash. Chem. 1982, 113, 699.
30. (b) Minelli, M.; Enemark, J. H.; Brownlee, R. T. C.; O'Connor, M. J.; Wedd, A. G. Coord. Chem. Rev. 1985, 68, 169.
31. (c) Mason, J. Chem. Rev. 1987, 87, 1299.
32. (a) Szymańska-Buzar, T. Coord. Chem. Rev. 2005, 249, 2195.
33. (b) Stosur, M; Górski, M.; Szymańska-Buzar, T. Unpublished results.
34. (a) Minato, M.; Yang, Z. D.; Zhang, L.-B.; Hirabayashi, R.; Kakeya, M.; Matsumoto, T.; Harakawa, A.; Kikutsuji, G.; Ito, T. Organometallics 2005, 24, 3434.
35. (b) Cugny, J.; Schmalle, H. W.; Fox, T.; Blacque, O.; Alfonso, M.; Berke, H. Eur. J. Inorg. Chem. 2006, 540.
36. (a) Matthews, S. L.; Pons, V.; Heinekey, D. M. Inorg. Chem. DOI, 10.1021/ic052134p.
37. (b) Ga̧dek, A.; Szymańska-Buzar, T. Polyhedron 2006, 25, 1441.
38. (a) Greene, J.; Curtis, M. D. Inorg. Chem. 1978, 17, 2324.
39. (b) Aitken, C.; Barry, J.-P.; Gauvin, F.; Harrod, J. F.; Malek, A.; Rousseau, D. Organometallics 1989, 8, 1732.
40. (c) Chang, L. S.; Corey, J. Y. Organometallics 1989, 8, 1885.
41. (a) Oxford Diffraction Poland Sp., CCD data collection and reduction GUI, Version 1.173.13 beta (release 14.11.2003), 1995-2003.
42. (b) Sheldrick, G. M. SHELXS-97, Program for Crystal Structure Solution; University of Göettingen: Germany, 1997.
43. (c) Sheldrick, G. M. SHELXL-97, Program for Crystal Structure Refinement, University of Göettingen: Germany, 1997.