Influence of temperature of silica gel activation on separation of selected biologically active steroid compounds

Journal of Liquid Chromatography and Related Technologies

Volumn 29, Issue 14, 2006, Pages 2035-2044

  Pyka, A ^a   Babuska, M ^a   Bober, K ^a   Gurak, D ^a   Klimczok, Wioletta ^a   Miszczyk, M ^b  

^a MEDICAL UNIVERSITY OF SILESIA   (Poland)

^b INSTITUTE OF PLANT PROTECTION NATIONAL RESEARCH INSTITUTE   (Poland)

Author keywords

Activation of silica gel; Drugs; Separation; Steroid compounds; Temperature; TLC

Indexed keywords

ACTIVATION ENERGY; ALCOHOLS; CHOLESTEROL; CHROMATOGRAPHIC ANALYSIS; DRUG PRODUCTS; KETONES; SEPARATION; TEMPERATURE CONTROL;

ACTIVATION OF SILICA GEL; SILICA GEL ACTIVATION; STEROID COMPOUNDS; TLC;

SILICA GEL;

ACETONE; ANDROSTERONE; CHLOROFORM; CHOLESTEROL; EPIANDROSTERONE; ESTRADIOL; HYDROCORTISONE; PRASTERONE; SILICA GEL; SITOSTEROL; STEROID; STIGMASTEROL; TESTOSTERONE;

ADSORPTION CHROMATOGRAPHY; ARTICLE; TEMPERATURE; THIN LAYER CHROMATOGRAPHY; TIME;

EID: 33746238951     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070600758449     Document Type: Article

References (15)

1. Kołodziejczyk, A. Natural Organic Compounds (in Polish); PWN: Warsaw, 2003.
2. Murray, R.K.; Granner, D.K.; Mayes, P.A.; Rodwell, V.W. Harper's Biochemistry (in Polish); PZWL: Warsaw, 1995.
3. Auranen, A.; Hietanen, S.; Salmi, T.; Grenman, S. Hormonal treatments and epithelial ovarian cancer risk. Intl. J. Gynecol. Cancer 2005, 15 (5), 692-700.
4. Rau, K.M.; Kang, H.Y.; Cha, T.L.; Miller, S.A.; Hung, M.C. The mechanisms and managements of hormone-therapy resistance in breast and prostate cancers. Endocr. Relat. Cancer 2005, 12 (3), 511-532.
5. Vasudevan, H.; Xiang, H.; McNeill, J.H. Differential regulation of insulin resistance and hypertension by sex hormones in fructose-fed male rats. Am. J. Physiol. Heart Circ. Physiol. 2005, 289 (4), H1335-H1342.
6. Liman, S.T.; Kara, C.O.; ir, F.; Yildirim, B.; Topcu, S.; Sahin, B. The effects of estradiol and progesterone on the synthesis of collagen in tracheal surgery. Intl. J. Pediatr. Otorhinolaryngol. 2005, 69 (10), 1327-1331.
7. Sugishita, K.; Uchida, M.; Ikeda, M.; Asakawa, M.; Sato, T.; Ito, N.; Hada, Y. Gender difference in subjective symptoms related to paroxysmal atrial fibrillation is also detected in postmenopausal women. Intl. Heart J. 2005, 46 (4), 669-678.
8. Recio, R.; Ocampo-Gomez, G.; Moran-Martinez, J.; Borja-Aburto, V.; Lopez-Cervante, M.; Uribe, M.; Torres-Sanchez, L.; Cebrian, M.E. Pesticide exposure alters follicle-stimulating hormone levels in Mexican agricultural workers. Environ. Health Perspect. 2005, 113 (9), 1160-1163.
9. Zhu, N.; Eghbali, M.; Helguera, G.; Song, M.; Stefani, E.; Toro, L. Alternative splicing of Slo channel gene programmed by estogen, progesterone and pregnancy. FEBS Lett. 2005, 579 (21), 4856-4860.
10. Tsolaki, M.; Grammaticos, P.; Karnasou, C.; Balaris, V.; Kapoukranidou, D.; Kalpidis, I.; Petsanis, K.; Dedousi, E. Serum estradiol, progesterone, testosterone, FSH and LH levels in postmenopausal women with Alzheimer's dementia. Hellenic J. Nucl. Med. 2005, 8 (1), 39-42.
11. Lepri, L.; Cincinelli, A.; Del Bubba, M. Reversed phase planar chromatography of optical isomers on microcrystaline cellulose triacetate. J. Planar Chromatogr.-Mod. TLC 1999, 12 (4), 298-301.
12. Śliwiok, J.; Kwapniewski, Z. Regularity of process of chromatographic separation of homologous series of higher fatty acids (in Polish). Pedagogical University in Katowice, Scientific book, Section of Chemistry 1963, 4, 47-50.
13. Pyka, A.; Bober, K. Investigation of a homologous series of fatty acids by TLC. Part III application of terms describing the separation of homologous series of saturated fatty acids in TLC. J. Planar Chromatogr.-Mod. TLC 2003, 16 (4), 303-307.
14. Pyka, A.; Dołowy, M. Separation of selected bile acids by TLC. I. J. Liq. Chromatogr. & Rel. Technol. 2003, 26 (7), 1095-1108.
15. Pyka, A.; Dołowy, M. Separation of selected bile acids by TLC. II. One-dimensional and two-dimensional TLC. J. Chromatogr. & Rel. Technol. 2004, 27 (13), 2031-2038.