Simple method for the preparation of dimethyl acetals from ketones with montmorillonite K 10 and p-toluenesulfonic acid

Synthetic Communications

Volumn 36, Issue 15, 2006, Pages 2195-2201

  Mansilla, Horacio ^a   Regás, David ^b  

^a INSTITUTO DE PRODUCTOS NATURALES Y AGROBIOLOGÍA   (Spain)

^b UNIVERSIDAD DE LA LAGUNA   (Spain)

Author keywords

Dimethyl acetals; Ketones; Montmorillonite K 10; p toluenesulfonic acid

Indexed keywords

ACETAL DERIVATIVE; DIMETHYL ACETAL; KETONE; MONTMORILLONITE; MONTMORILLONITE K 10; TOLUENESULFONIC ACID; TOLUENESULFONIC ACID DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CATALYST; REACTION ANALYSIS; SYNTHESIS; TECHNIQUE;

EID: 33745350377     PISSN: 00397911     EISSN: 15322432     Source Type: Journal    
DOI: 10.1080/00397910600639315     Document Type: Article

References (23)

1. (a) Green, T. W.; Wuts, P. G. M. Protective Groups in Organic Synthesis, 3rd ed; Wiley: New York, 1999;
2. (b) Meskens, F. A. J. Synthesis 1981, 501.
3. Wenkert, E.; Goodwin, T. E. Synth. Commun. 1970, 35, 3375.
4. Thurkauf, A.; Jacobson, A. E.; Rice, K. C. Synthesis 1988, 233.
5. Cameron, A. F. B.; Hunt, J. S.; Oughton, J. F.; Wilkinson, P. A.; Wilson, B. M. J. Chem. Soc. 1953, 3864.
6. Anderson, S. H.; Uh, H.-S. Synth. Commun. 1973, 3, 125.
7. Tsunoda, T.; Suzuki, M.; Noyori, R. Tetrahedron Lett. 1980, 21, 1357.
8. Gemal, A. L.; Luche, J.-L. J. Org. Chem. 1979, 44, 4187.
9. Ishihara, K.; Karumi, Y.; Kubota, M.; Yamamoto, H. Synlett 1996, 839.
10. Leonard, N. M.; Oswald, M. C.; Freiberg, D. A.; Nattier, B. A.; Smith, R. C.; Mohan, R. S. J. Org. Chem. 2002, 67, 5202.
11. Srivastava, N.; Dasgupta, S. K.; Banik, B. K. Tetrahedron Lett. 2003, 44, 1191.
12. Surya, K. D.; Gibbs, A. Tetrahedron Lett. 2004, 45, 8141.
13. Clerici, A.; Pastori, N.; Porta, O. Tetrahedron 2001, 57, 217.
14. Taylor, E. C.; Chiang, C.-S. Synthesis 1977, 467.
15. Corma, A.; Climent, M. J.; García, H.; Primo, J. Appl. Catal. 1990, 59, 333.
16. Olah, G. A.; Narang, S. C.; Mediar, D.; Salem, G. F. Synthesis 1981, 282.
17. Thomas, B.; Prathapan, S.; Sugunan, S. Micropor. Mesopor. Mat. 2005, 80, 65.
18. Tateiwa, J.; Horiuchi, H.; Uemura, S. J. Org. Chem. 1995, 60, 4039.
19. Tanaka, Y.; Sawamura, N.; Iwamoto, M. Tetrahedron Lett. 1998, 39, 9457.
20. Shimizu, K.; Hayashi, E.; Hatamachi, T.; Kodama, T.; Kitayama, Y. Tetrahedron Lett. 2004, 45, 5135.
21. (a) Oshima, T.; Nishioka, R.; Nagai, T. Tetrahedron Lett. 1980, 21, 3919;
22. (b) Oshima, T.; Nagai, T. J. Org. Chem. 1989, 54, 1465.
23. Karimi, B.; Ashtiani, A. M. Chem. Lett. 1999, 1199.