Recrystallization of CL-20 and HNFX from solution for rigorous control of the polymorph type: Part II, Experimental studies

Journal of Energetic Materials

Volumn 24, Issue 2, 2006, Pages 103-139

  Degirmenbasi, N ^a   Peralta Inga, Z ^a   Olgun, U ^a   Gocmez, H ^a   Kalyon, D M ^a  

^a STEVENS INSTITUTE OF TECHNOLOGY   (United States)

Author keywords

CL 20; Conventional crystallization; HNFX; Micro crystallization; Polymorph analysis; Powder diffraction; Rietveld analysis

Indexed keywords

EID: 33745138779     PISSN: 07370652     EISSN: 15458822     Source Type: Journal    
DOI: 10.1080/07370650600672090     Document Type: Article

References (13)

1. Kamlet, M. J. and S. J. Jacobs. 1968. Chemistry of detonations, i. a simple method for calculating detonation properties of C-H-N-O explosives. J. Chem. Phys., 48: 23-36.
2. Chapman,R. D.,R. D. Gilardi,M. F. Welker, and C. B. Kreutzberger. 1999. Nitrolysis of a highly deactivated amide by protonitronium. synthesis and structure of HNFX. J. Org. Chem., 64: 960.
3. Philip F. Pagoria, Gregory S. Lee, Alexander R. Mitchell, and Robert D. Schmidt. 2002. A review of energetic materials synthesis. Thermochimica Acta., 384: 187-204.
4. von Holtz, E., D. Ornellas, M. F. Foltz, and J. E. Clarkson. 1994. The solubility of ε-CL-20 in selected materials propellants, explosives. Pyrotechnics, 19: 206-212.
5. Mullin, J. W. 1997. Crystallization. Oxford, UK: Butterworth Heinemann.
6. Liapis, S.A. 1998. Modeling of the primary and secondary drying stages of the freeze drying of pharmaceutical products in vials: numerical results obtained from the solution of a dynamic and spatially multi-dimensional lyophilization model for different operational policies. Biotechnology and Bioengineering, 60, 6: 712-728.
7. Snowman, J. W. 1988. Downstream Processes: Equipment and Techniques, pp. 315-351, Alan R. Liss, Inc.
8. Myerson, A. S. (Ed.). 2002. Handbook of Industrial Crystallization. Boston, USA: Butterworth Heinemann.
9. Davey, R. J. 1982. In S. J. Jancic (ed.), Industrial Crystallization 81, pp. 431-479, Amsterdam: North-Holland publishing Co.
10. Lia Addadi, Ziva Berkovitch-Yellin, Isabelle Weissbuch, Jan van Mil, Linda J. W. Shimon, Meir Lahav, and Leslie Leiserowitz. 1985. Growth and dissolution of organic crystals with "tailor-made." Inhibitors-Implications in Stereochemistry and Materials Science, 24, 6: 466-485.
11. Caddick, S. 1995. Microwave assisted organic reactions. Tetrahedron, 51: 10403-10432.
12. Loupy, A., A. Petit, J. Hamelin, F. Texier-Boullet, P. Jacquault, and D. Mathe. 1998. Synthesis. New Solvent-Free Organic Synthesis Using Focused Microwaves, 9: 1231-1234.
13. Bose, A. K., M. S. Manhas, R. K. Banik, and E. W. Robb. 1994. Microwave-induced organic reaction enhancement (more) chemistry: techniques for rapid, safe and inexpensive synthesis. Res. Chem. Intermed, 20, 1: 1-11.