Apolar chromatography on Sephadex LH-20 combined with high-speed counter-current chromatography. High yield strategy for structurally closely related analytes-Destruxin derivatives from Metarhizium anisopliae as a case study

Journal of Chromatography A

Volumn 1117, Issue 1, 2006, Pages 67-73

  Seger, Christoph ^a   Eberhart, Karin ^a,b   Sturm, Sonja ^a   Strasser, Hermann ^b   Stuppner, Hermann ^a  

^a INNSBRUCK MEDICAL UNIVERSITY   (Austria)

^b UNIVERSITY OF INNSBRUCK   (Austria)

Author keywords

Destruxins; High speed counter current chromatography; HSCCC; Metarhizium anisopliae; Sephadex LH20

Indexed keywords

CELL CULTURE; COLUMN CHROMATOGRAPHY; DERIVATIVES; EXTRACTION; METHANOL; PURIFICATION;

DESTRUXINS; HSCCC; METARHIZIUM ANISOPLIAE; SEPHADEX-LH20;

GELS;

ACETIC ACID ETHYL ESTER; DESTRUXIN; DESTRUXIN A; DESTRUXIN B; DESTRUXIN D; DESTRUXIN E; METHANOL; PEPTIDE DERIVATIVE; PETROLEUM; SEPHADEX; UNCLASSIFIED DRUG; WATER;

ARTICLE; CHEMICAL PROCEDURES; COLUMN CHROMATOGRAPHY; COUNTER CURRENT CHROMATOGRAPHY; FUNGUS CULTURE; LIPOPHILICITY; LIQUID LIQUID EXTRACTION; METARHIZIUM ANISOPLIAE; PRIORITY JOURNAL; PURIFICATION; SEPARATION ANXIETY;

ASCOMYCOTA; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, ION EXCHANGE; COUNTERCURRENT DISTRIBUTION;

FUNGI; METARHIZIUM ANISOPLIAE;

EID: 33646270623     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2006.03.055     Document Type: Article

References (46)

1. Cordell G.A., and Shin Y.G. Pure Appl. Chem. 6 (1999) 1089
2. Hostettmann K., Marston A., and Hostettmann M. Preparative Chromatography Techniques: Applications in Natural Product Isolation (1986), Springer-Verlag, Berlin
3. Hostettmann K., and Marston A. Phytochem. Rev. 1 (2002) 275
4. Verpoorte R., Contin A., and Memelink J. Phytochem. Rev. 1 (2002) 13
5. Seger C., Sturm S., Stuppner H., Butt T.M., and Strasser H. J. Chromatogr. A 1061 (2004) 35
6. Pedras M.S.C., Zaharia I.L., and Ward D.E. Phytochemistry 59 (2002) 579
7. Vey A., Hoagland R., and Butt T.M. In: Butt T.M., Jackson C.W., and Magan N. (Eds). Fungi as Biocontrol Agents: Progress, Problems and Potential (2001), CAB International, Wallingford 311
8. Païs M., Das B.C., and Ferron P. Phytochemistry 20 (1981) 715
9. Samuels R.I., Charnley A.K., and Reynolds S.E. Mycopathologica 104 (1988) 51
10. Gupta S., Roberts D.W., and Renwick J.A.A. J. Liq. Chromatogr. 12 (1989) 383
11. Buchwaldt L., and Jensen J.S. Phytochemistry 30 (1991) 2311
12. Wahlmann M., and Davidson B.S. J. Nat. Prod. 56 (1991) 643
13. Jegorov A., Matha V., Sedmera P., and Roberts D.W. Phytochemistry 31 (1992) 2669
14. Krasnoff S.B., Gibson D.M., Belofsky G.N., Gloer K.B., and Gloer J.B. J. Nat. Prod. 59 (1996) 485
15. Jegorov A., Sedmera P., Havlicek V., and Matha V. Phytochemistry 49 (1998) 1815
16. Chen J.W., Liu B.L., and Tzeng Y.M. J. Chromatogr. A 830 (1999) 115
17. Faulstich H., Buku A., Bodenmüller H., and Wieland T. Biochemistry 19 (1980) 3334
18. Henke H. LaborPraxis 11 (1987) 644
19. Henke H. Preparative Gel Chromatography on Sephadex LH-20 (1996), Huethig, Heidelberg
20. Kubanek J., Hay M.E., Brown P.J., Lindquist N., and Fenical W. Chemecology 11 (2001) 1
21. Jongaramruong J., Blackman A.J., Skelton B.W., and White A.H. Aust. J. Chem. 55 (2002) 275
22. Riepe F.G., Krone N., Peter M., Sippell W.G., and Partsch C.J. J. Chromatogr. B 785 (2003) 293
23. Du Q., Jerz G., Chen P., and Winterhalter P. J. Liq. Chromatogr. Rel. Technol. 27 (2004) 2201
24. Du Q., Jerz G., and Winterhalter P. J. Chromatog. A 1045 (2004) 59
25. Wei Y., Zhang T., and Ito Y. J. Chromatogr. A 1033 (2004) 373
26. Cao X., Dong Y., Zhao H., Pan X., and Ito Y. J. Liq. Chromatogr. Rel. Technol. 28 (2005) 2005
27. Schaefer K., and Winterhalter P. J. Liq. Chromatogr. Rel. Technol. 28 (2005) 1703
28. Wang X., Fuwei L., Qinglei S., Jingpeng Y., Ting Y., and Chengchao Z. J. Chromatogr. A 1063 (2005) 247
29. Aman R., Carle R., Conrad J., Beifuss U., and Schieber A. J. Chromatogr. A 1074 (2005) 99
30. Wang-Fan W., Kusters E., Lohse O., Mak C.P., and Wang Y. J. Chromatogr. A 864 (1999) 69
31. Wang-Fan W., Kusters E., Mak C.P., and Wang Y. J. Liq. Chromatogr. Rel. Technol. 23 (2000) 1365
32. Wang-Fan W., Kusters E., Mak C.P., and Wang Y. Chromatogr. A 925 (2001) 139
33. Fang D., Xie Y., Chen Y., Chen X., and Zheng W. Zhongguo Kangshengsu Zazhi 30 (2005) 48
34. Ito Y. J. Chromatogr. A 1065 (2005) 145
35. Ito Y. CRC Crit. Rev. Anal. Chem. 17 (1986) 65
36. Chen L.J., Song H., Lan X.Q., Games D.E., and Sutherland I.A. J. Chromatogr. A 1063 (2005) 241
37. Liu C.M., Huang S.S., and Tzeng Y.M. J. Chromatogr. Sci. 42 (2004) 140
38. Jegorov A., Paisz B., Zabka M., Kuzma M., Havlicek V., Giannakopulos A.E., and Derrick P.J. Eur. J. Mass Spectrom. 9 (2003) 105
39. Jegorov A., Havlicek V., and Sedmera P. J. Mass Spectrom. 33 (1998) 274
40. Seger C., Sturm S., Strasser E.M., Ellmerer E.P., and Stuppner H. Magn. Reson. Chem. 42 (2004) 882
41. Wang C., Skrobek A., and Butt T.M. J. Invertebr. Pathol. 85 (2004) 68
42. Loutelier C., Cherton J.C., Lange C., Traris M., and Vey A. J. Chromatogr. A 738 (1996) 181
43. Wahlman M., and Davidson B.S. J. Nat. Prod. 56 (1993) 643
44. Dudley E., Wang C., Skrobek A., Newton R.P., and Butt T.M. Rapid Commun. Mass Spectrom. 18 (2004) 2577
45. Gupta S., Roberts D.W., and Renwick J.A.A. J. Chem. Soc.: Perkin Trans. 1 (1989) 2347
46. Ward D.E., Gai Y., Lazny R., and Pedras M.S.C. J. Org. Chem. 66 (2001) 7832