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33645824871
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note
-
2 data (SHELXL-97, 550 parameters with no restraints), with R1 = 0.0586 and wR2 = 0.1185 (all data).
-
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-
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33
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33645803321
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note
-
The reactions slowed at lower temperatures.
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-
-
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34
-
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33645818879
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note
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1H NMR spectrum of the free ligand at -60 °C shows only signals of the cone conformer. See also ref 2.
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36
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