Inductively coupled plasma optical emission spectrometric determination of gadolinium in urine using flow injection on-line sorption preconcentration in a knotted reactor

Instrumentation Science and Technology

Volumn 34, Issue 3, 2006, Pages 305-316

  Salonia, J A ^a   Gasquez J A ^a   Martinez, L D ^a   Cerutti, S ^b   Kaplan, M ^b   Olsina, R A ^b  

^a UNIVERSIDAD NACIONAL DE SAN LUIS   (Argentina)

^b Universidad Nacional de Río Cuarto Consejo Nacional de Investigaciones Científicas y Técnicas   (Argentina)

Author keywords

Gadolinium determination; ICP OES; Knotted reactor; On line preconcentration; Urine samples

Indexed keywords

BODY FLUIDS; CONCENTRATION (PROCESS); EMISSION SPECTROSCOPY; LIGHT EMISSION; NITRIC ACID; SORPTION; ULTRASONICS;

GADOLINIUM DETERMINATION; INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES); KNOTTED REACTORS; ON-LINE PRECONCENTRATION; RELATIVE STANDARD DEVIATION (RSD); URINE SAMPLES;

GADOLINIUM;

EID: 33645766062     PISSN: 10739149     EISSN: 15256030     Source Type: Journal    
DOI: 10.1080/10739140600605910     Document Type: Article

References (33)

1. Seiler, H.G.; Sigel, A.; Sigel, H. Handbook on Metals in Clinical and Analytical Chemistry; Marcel Dekker, Inc.: New York, 1994; 354.
2. Evans, C.H. Biochemistry of the Lanthanides; Plenum Press: New York, 1990.
3. Platas-Iglesias, C.; Mato-Iglesias, M.; Djanashvili, K.; Muller, R.N.; Elst, L.V.; Peters, J.A.; Blas, A.; Rodriguez-Blas, T. Lanthanide chelates containing piridine units with potential application as contrast agents in magnetic resonance imaging. Chemistry 2004, 19, 3579-3590.
4. Kostova, I.; Manolov, I.; Momekov, G. Cytotoxic activity of new neodymium(III) complexes of bis-coumarins. Eur. J. Med. Chem. 2004, 39, 765-777.
5. Koudriavtseva, T.; Thompson, A.J.; Fiorelli, M.; Gasperini, C.; Bastianello, S.; Bozzao, A.; Paolillo, A.; Pisani, A.; Galgani, S.; Pozzilli, C. Gadolinium enhanced MRI predicts clinical and MRI disease activity in relapsing/remitting multiple sclerosis. J. Neurol. Neurosurg., Psychiatry 1997, 62, 285-287.
6. Mayoral, E.P.; García-Amo, M.; López, P.; Soriano, E.; Cerdán, S.; Ballesteros, P. A novel series of complexones with bis- or biazole structure as mixed ligands of paramagnetic contrast agents for MRI. Bioorg. Med. Chem. 2003, 11, 5555-5567.
7. Naganawa, S.; Nihashi, T.; Fukatsu, H.; Ishigaki, T.; Aoki, I. Pre-surgical mapping of primary motor cortex by functional MRI at T: effects of intravenous administration of Gd-DTPA. Eur. Radiol. 2004, 14, 112-114.
8. Loreti, V.; Bettmer, J. Determination of the MRI contrast agent Gd-DTPA by SECICP-MS. Anal. Bioanal. Chem. 2004, 379, 1050-1054.
9. Feng, J.; Sun, G.; Pei, F.; Liu, M. Comparison between Gd-DTPA and several bisamide derivatives as potential MRI contrast agents. Bioorg. Med. Chem. 2003, 11, 3359-3366.
10. Colosimo, C.; Knopp, M.V.; Barreau, X.; Gerardin, E.; Kirchin, M.A.; Guezenoc, F.; Lodemann, K.P. A comparison of Gd-BOPTA and Gd-DOTA for contrast-enhanced MRI of intracranial tumors. Neuroradiology 2004, 46, 655-665.
11. Canet, E.P.; Casali, C.; Desenfant, A.; An, M.Y.; Corot, C.; Obadia, J.F.; Revel, D.; Janier, M.I. Kinetic characterization of CMD-A2-Gd-DOTA as an intravascular contrast agent for myocardial perfusion measurement with MRI. Magn. Reson. Med. 2000, 43, 403-409.
12. Bunzli, C.G.; Choppin, G.R. Lanthanide Probes in Life, Chemical and Earth Sciences; Elsevier: Amsterdam, 1989; Chapter 5.
13. Galli, P.; Oddo, N. Ultrasonic nebulization in inductively coupled plasma atomic emission spectrometry. Microchem. J. 1992, 46, 327-334.
14. Sun, D.A.; Waters, J.; Mawhinney, T. Microwave digestion and ultrasonic nebulization for determination of boron in animal tissues by inductively coupled plasma atomic emission spectrometry with internal standardization and addition of mannitol. J. Anal. Atom. Spectrom. 1997, 12, 675-679.
15. Hoenig, M.; Baeten, H.; Vanhentenrijk, S.; Ploegaerts, T.; Bertholet, T. Evaluation of various commercially available nebulizers for inductively coupled plasma atomic emission spectrometry. Analusis 1997, 25, 13-19.
16. Silva, M.F.; Fernández, L.P.; Olsina, R.A. Monitoring the elimination of gadolinium-based pharmaceuticals cloud point preconcentration and spectrophotometric determination of Gd(III)-2-(3,5-dichloro-2-pyridylazo)-5- dimethylaminophenol in urine. Analyst 1998, 123, 1803-1807.
17. Ortega, C.; Gómez, M.R.; Olsina, R.A.; Silva, M.F.; Martinez, L.D. On-line cloud point preconcentration and determination of gadolinium in urine using flow injection inductively coupled plasma optical emission spectrometry. J. Anal. Atom. Spectrom. 2002, 17, 530-533.
18. Devito, I.E.; Olsina, R.A.; Raba, J.; Massi, A.N. Flow injection preconcentration by chemofiltration and spectrophotometric determination of Gd. Anal. Chim. Acta 2004, 507, 11-16.
19. Yang, X-P.; Li, V.; Jiang, Y. A flow injection on-line displacement/sorption preconcentration and separation technique coupled with flame atomic absorption spectrometry for the determination of trace copper in complicated matrices. J. Anal. Atom. Spectrom. 2002, 17, 610-615.
20. Dittfurth, C.; Ballesteros, E.; Gallego, M.; Valcárcel, M. On-line precipitation/ dissolution system for the preconcentration and determination of manganese traces by atomic absorption spectrometry. Spectrochim. Acta B 1996, 51, 1935-1941.
21. Ivanova, E.; Yan, X.P.; Adams, F. Determination of bismuth in cod muscle, lake and river sediment by flow injection on-line sorption preconcentration in a knotted reactor coupled with electrothermal atomic absorption spectrometry. Anal. Chim. Acta 1997, 354, 1-13.
22. Ivanova, E.; Adams, F. Flow injection on-line sorption preconcentration of platinum in a knotted reactor coupled with electrothermal atomic absorption spectrometry. Fresen. J. Anal. Chem. 1998, 361, 445-450.
23. Nielsen, S.; Hansen, E.H. Selective flow-injection quantification of ultra-trace amounts of Cr(VI) via on-line complexation and preconcentration with APDC followed by determination by electrothermal atomic absorption spectrometry. Anal. Chim. Acta 1998, 366, 163-176.
24. Ivanova, E.; Benkhedda, K.; Adams, F. Determination of copper, manganese and nickel in biological samples and sea-water by flow injection on-line sorption preconcentration in a knotted reactor coupled with electrothermal atomic absorption spectrometry. J. Anal. Atom. Spectrom. 1998, 13, 527-531.
25. Benkhedda, K.; Ivanova, E.; Adams, F. Row injection on-line sorption preconcentration of trace amounts of copper and manganese in a knotted reactor precoated with 1-phenyl-3-methyl-4-benzoylpyrazol-5-one coupled with electrothermal atomic absorption spectrometry. J. Anal. Atom. Spectrom. 1999, 14, 957-961.
26. Salonia, J.A.; Wuilloud, R.G.; Gásquez, J.A.; Olsina, R.A.; Martinez, L.D. Determination of lead in tap water by ICP-AES with flow-injection on-line adsorption preconcentration using a knotted reactor and ultrasonic nebulization. J. Anal. Atom. Spectrom. 1999, 14, 1239-1243.
27. Salonia, J.A.; Wuilloud, R.G.; Gásquez, J.A.; Olsina, R.A.; Martinez, L.D. On-line complexation of zinc with 5-Br-PADAP and preconcentration using a knotted reactor for inductively coupled plasma atomic emission spectrometric determination in river water samples. Fresen. J. Anal. Chem. 2000, 367, 653-657.
28. Wuilloud, R.G.; Salonia, J.A.; Olsina, R.A.; Martinez, L.D. Determination of vanadium(V) in drinking water by flow injection and pre-concentration in a knotted reactor by inductively coupled plasma optical emission spectrometry with ultrasonic nebulization. Spectrochim. Acta B 2000, 55, 671-680.
29. Lara, R.F.; Wuilloud, R.G.; Salonia, J.A.; Olsina, R.A.; Martinez, L.D. Determination of low cadmium concentrations in wine by on-line preconcentration in a knotted reactor coupled to an inductively coupled plasma optical emission spectrometer with ultrasonic nebulization. Fresen. J. Anal. Chem. 2001, 371, 989-993.
30. Sperling, M.; Yan, X.; Welz, B. Investigation of on-line coupling electrothermal atomic absorption spectrometry with flow injection sorption preconcentration using a knotted reactor for totally automatic determination of lead in water samples. Spectrochim. Acta B 1996, 57, 1891-1908.
31. Moyano, S.; Wuilloud, R.G.; Olsina, R.A.; Gásquez, J.A.; Martinez, L.D. On-line preconcentration system for bismuth determination in urine by flow injection hydride generation inductively coupled plasma atomic emission spectrometry. Talanta 2001, 54, 211-219.
32. Crock, J.C.; Lichte, F.E.; Riddle, G.O.; Beech, C.L. Separation and preconcentration of the rare-earth elements and yttrium from geological materials by ionexchange and sequential acid elution. Talanta 1986, 33, 601-606.
33. Allain, P.; Berre, S.; Premel-Cabic, A.; Mauras, Y.; Delaporte, T. Concentrations of rare earth elements in plasma and urine of healthy subjects determined by inductively coupled plasma mass spectrometry. Clin. Chem. 1990, 36, 2011-2012.