Activation of a Cu/ZnO catalyst for methanol synthesis

Journal of Applied Crystallography

Volumn 39, Issue 2, 2006, Pages 209-221

  Andreasen, Jens Wenzel ^a   Rasmussen, Frank Berg ^b,c   Helveg, Stig ^b   Molenbroek, Alfons ^b   Ståhl, Kenny ^a   Nielsen, Martin Meedom ^a   Feidenhans'l, Robert ^a,d  

^a TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

^b HALDOR TOPSØE A S   (Denmark)

^c Haldor Topsøe A/S ^*  (Denmark)

^d UNIVERSITY OF COPENHAGEN   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33645133252     PISSN: 00218898     EISSN: 16005767     Source Type: Journal    
DOI: 10.1107/S0021889806003098     Document Type: Article

References (70)

1. Albertsson, J., Abrahams, S. C. & Kvick, Å. (1989). Acta Cryst. B45, 34-40.
2. Andreasen, J. W., Rasmussen, O., Feidenhans'l, R., Rasmussen, F. B., Christensen, R., Molenbroek, A. M. & Goerigk, G. (2003). J. Appl. Cryst. 36, 812-813.
3. Bazin, D., Guczi, L. & Lynch, J. (2002). Appl. Catal. A Gen. 226, 87-113.
4. Burch, R., Golunski, S. & Spencer, M. S. (1990). Catal. Lett. 5, 55-60.
5. Chinchen, G. C., Waugh, K. C. & Whan, D. A. (1986). Appl. Catal. 25, 101-107.
6. Choi, Y., Futagami, K., Fujitani, T. & Nakamura, J. (2001). Catal. Lett. 73, 27-31.
7. Clausen, B. S., Schiøtz, J., Gråbæk, L., Ovesen, C. V., Jacobsen, K. W., Nørskov, J. K. & Topsøe, H. (1994). Top. Catal. 1, 367-375.
8. Clausen, B. S., Steffensen, G., Fabius, B., Villadsen, J., Feidenhans'l, R. & Topsøe, H. (1991). J. Catal. 132, 524-535.
9. Cromer, D. T. & Liberman, D. (1970). J. Chem. Phys. 53, 1891-1898.
10. Cross, J. O., Newville, M., Rehr, J. J., Sorensen, L. B., Bouldin, C. E., Watson, G., Couder, T., Lander, G. H. & Bell, M. I. (1998). Phys. Rev. B, 58, 11215-11225.
11. Derouane, E. G., Chludzinski, J. J. & Baker, R. T. K. (1984). J. Catal. 85, 187-196.
12. Egerton, R. F. (1996). Electron Energy-Loss Spectroscopy in the Electron Microscope, 2nd ed. Dordrecht: Kluwer Academic/ Plenum.
13. Frederick, M. J. & Ramanath, G. (2004). J. Appl. Phys. 95, 3202-3205.
14. Fujitani, T. & Nakamura, J. (2000). Appl. Catal. A, 191, 111-129.
15. Golub, G. H. & Reinsch, C. (1970). Numer. Math. 14, 403-420.
16. Greeley, J., Gokhale, A. A., Kreuser, J., Dumesic, J. A., Topsoe, H., Topsoe, N. Y. & Mavrikakis, M. (2003). J. Catal. 213, 63-72.
17. Grunwaldt, J. D., Molenbroek, A. M., Topsøe, N. Y., Topsøe, H. & Clausen, B. S. (2000). J. Catal. 194, 452-460.
18. Günter, M. M., Bems, B., Schlogl, R. & Ressler, T. (2001). J. Synchrotron Rad. 8, 619-621.
19. Günter, M. M., Ressler, T., Bems, B., Buscher, C., Genger, T., Hinrichsen, O., Muhler, M. & Schlogl, R. (2001). Catal. Lett. 71, 37-44.
20. Hadden, R. A., Sakakini, B., Tabatabaei, J. & Waugh, K. C. (1997). Catal. Lett. 44, 145-151.
21. Hansen, P. L., Wagner, J. B., Helveg, S., Rostrup-Nielsen, J. R., Clausen, B. S. & Topsoe, H. (2002). Science, 295, 2053-2055.
22. Haubold, H. G., Gruenhagen, K., Wagener, M., Jungbluth, H., Heer, H., Pfeil, A., Rongen, H., Brandenberg, G., Moeller, R., Matzerath, J., Hiller, P. & Hailing, H. (1989). Rev. Sci. Instrum. 60, 1943-1946.
23. Hodeau, J. L., Favre-Nicolin, V., Bos, S., Renevier, H., Lorenzo, E. & Berar, J. F. (2001). Chem. Rev. 101, 1843-1867.
24. Iraji-zad, A., Ahadian, M. M. & Vashaei, Z. (2002). J. Phys. D Appl. Phys. 35, 1176-1182.
25. Istratov, A. A., Hedemann, H., Seibt, M., Vyvenko, O. F., Schroter, W., Heiser, T., Flink, C., Hieslmair, H. & Weber, E. R. (1998). J. Electrochem. Soc. 145, 3889-3898.
26. Ketchik, S. V., Minyukova, T. P., Kuznetsova, L. I., Plyasova, L. M., Yurieva, T. M. & Boreskov, G. K. (1982). React. Kinet. Catal. Lett. 19, 345-349.
27. Klenov, D. O., Kryukova, G. N. & Plyasova, L. M. (1998). J. Mater. Chem. 8, 1665-1669.
28. Konarev, P. V., Volkov, V. V., Sokolova, A. V., Koch, M. H. J. & Svergun, D. I. (2003). J. Appl. Cryst. 36, 1277-1282.
29. Konarev, P. V., Volkov, V. V. & Svergun, D. I. (2004). MIXTURE. Version 2.3. European Molecular Biology Laboratory, Hamburg Outstation.
30. Kronig, R. D. L. & Kramers, H. A. (1928). Z. Phys. 48, 174-179.
31. Krumm, S. (1994). Acta Univ. Carol. Geol. 38, 253-261.
32. Langford, J. I. (1999). Defect and Microstructure Analysis by Diffraction, edited by R. L. Snyder, J. Fiala & H. J. Bunge, pp. 59-81. Oxford University Press.
33. Langford, J. I., Boultif, A., Auffredic, J. P. & Louer, D. (1993). J. Appl. Cryst. 26, 22-33.
34. Larson, A. C. & Von Dreele, R. B. (2000). General Structure Analysis System (GSAS). Report LAUR 86-748. Los Alamos National Laboratory, NM, USA.
35. Le Bail, A., Duroy, H. & Fourquet, J. L. (1988). Mater. Res. Bull. 23, 447-452.
36. Mehta, S., Simmons, G. W., Klier, K. & Herman, R. G. (1979). J. Catal. 57, 339-360.
37. Okamoto, Y., Fukino, K., Imanaka, T. & Teranishi, S. (1983). J. Phys. Chem. 87, 3747-3754.
38. Ovesen, C. V., Clausen, B. S., Schiotz, J., Stoltze, P., Topsøe, H. & Norskov, J. K. (1997). J. Catal. 168, 133-142.
39. Patterson, B. D., Abela, R., Auderset, H., Chen, Q., Fauth, F., Gozzo, F., Ingold, G., Kuhne, H., Lange, M., Maden, D., Meister, D., Pattison, P., Schmidt, T., Schmitt, B., Schulze-Briese, C., Shi, M., Stampanoni, M. & Willmott, P. R. (2005). Nucl. Instrum. Methods Phys. Res. Sect. A, 540, 42-67.
40. Plyasova, L. M. (1996). Fourth European Powder Diffraction Conference, Vol. 228, Parts 1 and 2, pp. 341-346.
41. Plyasova, L. M., Molina, I. Y., Krieger, T. A., Davydova, L. P. & Yurieva, T. M. (2000). J. Mol. Catal. A Chem. 158, 331-336.
42. Plyasova, L. M., Solovyeva, L. P., Krieger, T. A., Makarova, O. V. & Yurieva, T. M. (1996). J. Mol. Catal. A Chem. 105, 61-66.
43. Plyasova, L. M., Yurieva, T. M., Molina, I. Y., Kriger, T. A., Balagurov, A. M., Davydova, L. P., Zaikovskii, V. I., Kustova, G. N., Malakhov, V. V. & Dovlitova, L. S. (2000). Kinet. Catal. 41, 429-436.
44. Poels, E. K. & Brands, D. S. (2000). Appl. Catal. A, 191, 83-96.
45. Polizzi, S., Riello, P., Goerigk, G. & Benedetti, A. (2002). J. Synchrotron Rad. 9, 65-70.
46. Rasmussen, B. S., Højlund Nielsen, P. E., Villadsen, J. & Hansen, J. B. (1987). Preparation of Catalysts IV, edited by B. Delmon, P. Grange, P. A. Jacobs & G. Poncelet, pp. 785. Amsterdam: Elsevier.
47. Rasmussen, P. B., Holmblad, P. M., Askgaard, T., Ovesen, C. V., Stoltze, P., Norskov, J. K. & Chorkendorff, I. (1994). Catal. Lett. 26, 373-381.
48. Robertus, C., Philipse, W. H., Joosten, J. G. H. & Levine, Y. K. (1989). J. Chem. Phys. 90, 4482-4490.
49. Samant, M. G., Bergeret, G., Meitzner, G. & Boudart, M. (1988). J. Phys. Chem. 92, 3542-3546.
50. Sasaki, S. (1989). Numerical Tables of Anomalous Scattering Factors. Calculated by the Cromer and Liberman Method. Report 88-14. KEK, Tsukuba, Ibaraki, Japan.
51. Satterfield, C. N. (1980). Heterogeneous Catalysis in Practice. New York: McGraw-Hill.
52. Schulz, G. V. (1939). Z. Phys. Chem. B, 43, 25.
53. Spencer, M. S. (1998). Catal. Lett. 50, 37-40.
54. Stephens, P. W. (1999). J. Appl. Cryst. 32, 281-289.
55. Stirling, D., Stone, F. S. & Spencer, M. S. (1993). Stud. Surf. Sci. Catal. 75, 1507-1518.
56. Stokes, A. R. (1948). Proc. Phys. Soc. London, 61, 382-391.
57. Svergun, D. I., Konarev, P. V., Volkov, V. V., Koch, M. H. J., Sager, W. F. C., Smeets, J. & Blokhuis, E. M. (2000). J. Chem. Phys. 113, 1651-1665.
58. Templeton, L. K. & Templeton, D. H. (1988). J. Appl. Cryst. 21, 558-561.
59. Toby, B. H. (2001). J. Appl. Cryst 34, 210-213.
60. Topsøe, N. Y. & Topsøe, H. (1999). J. Mol. Catal. A Chem. 141, 95-105.
61. Vegard, L. (1921). Z. Phys. 5, 17.
62. Wagner, J. B., Hansen, P. L., Molenbroek, A. M., Topsoe, H., Clausen, B. S. & Helveg, S. (2003). J. Phys. Chem. B, 107, 7753-7758.
63. Warren, B. E. (1969). X-ray Diffraction, pp. 251-314. Reading, MA: Addison-Wesley.
64. Williamson, G. K. & Hall, W. H. (1953). Acta Metall, 1, 22-31.
65. Wilson, A. J. C. (1962a). X-ray Optics. The Diffraction of X-rays by Finite and Imperfect Crystals, pp. 76-96. London: Methuen.
66. Wilson, A. J. C. (1962b). X-ray Optics. The Diffraction of X-rays by Finite and Imperfect Crystals, pp. 37-54. London: Methuen.
67. Yoshihara, J. & Campbell, C. T. (1996). J. Catal. 161, 776-782.
68. Yurieva, T. M., Plyasova, L. M., Kriger, T. A. & Makarova, O. V. (1995). Kinet. Catal. 36, 707-711.
69. Yurieva, T. M., Plyasova, L. M., Kriger, T. A., Zaikovskii, V. I., Makarova, O. V. & Minyukova, T. P. (1993). React. Kinet. Catal. Lett. 51, 495-500.
70. Yurieva, T. M., Plyasova, L. M., Zaikovskii, V. I., Minyukova, T. P., Bliek, A., van den Heuvel, J. C., Davydova, L. P., Molina, I. Y., Demeshkina, M. P., Khassin, A. A. & Batyrev, E. D. (2004). Phys. Chem. Chem. Phys. 6, 4522-4526.