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note
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int = 0.0387), R1 = 0.0264, wR2 = 0.0629. The H atoms were not located. The final cycles of least-squares refinement included atomic coordinates and anisotropic thermal parameters for all atoms.
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14
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33645075796
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note
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int = 0.0688), R1 = 0.0311, wR2 = 0.0760. The H atoms were located from difference Fourier maps. The final cycles of least-squares refinement included atomic coordinates and anisotropic thermal parameters for all non-H atoms. The atomic coordinates and isotropic thermal parameters for H atoms were fixed.
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