Synthesis of macrocycles containing two pyridine and two polyamine moieties via Pd-catalyzed amination

Tetrahedron Letters

Volumn 47, Issue 16, 2006, Pages 2691-2694

  Averin, Alexei D ^a   Ulanovskaya, Olesya A ^a   Borisenko, Anatolii A ^a   Serebryakova, Marina V ^b   Beletskaya, Irina P ^a  

^a MOSCOW STATE UNIVERSITY   (Russian Federation)

^b INSTITUTE OF BIOMEDICAL CHEMISTRY   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

2,6 DIHALOPYRIDINE DERIVATIVE; AMINE; DIOXADIAMINE; HALOGEN; MACROCYCLIC COMPOUND; PALLADIUM; POLYAMINE; PYRIDINE; PYRIDINE DERIVATIVE; UNCLASSIFIED DRUG;

AMINATION; ARTICLE; CATALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; COMPLEX FORMATION; SYNTHESIS;

EID: 33644986231     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2006.02.095     Document Type: Article

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12. 2 (8-13 mol %), BINAP (9-14 mol %) in abs. dioxane (20 ml) and sodium tert-butoxide (1.5 mmol) were added and the reaction mixture was refluxed for 10 h. Column chromatography was carried out using the sequence of eluents described for Method A.
13. +.