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Volumn 43, Issue 44, 2002, Pages 7945-7948

Preparation of new type of azacalixarene, azacalix[n](2,6)pyridine

Author keywords

Amination; Macrocycle; Palladium complex; Zinc complex

Indexed keywords

2 BROMO 6 (METHYLAMINO)PYRIDINE; 2,6 BIS(METHYLAMINO)PYRIDINE; 2,6 DIBROMOPYRIDINE; AZACALIX[4](2,6)PYRIDINE; AZACALIX[6](2,6)PYRIDINE; CALIXARENE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; PYRIDINE DERIVATIVE; UNCLASSIFIED DRUG;

EID: 0037190873     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(02)01842-7     Document Type: Article
Times cited : (99)

References (32)
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    • For reviews, see: (a) Böhmer, V. Angew. Chem., Int. Ed. Engl. 1995, 34, 713-745; (b) Ikeda, A.; Shinkai, S. Chem. Rev. 1997, 97, 1713-1734; (c) Weiser, C.; Dieleman, C. B.; Matt, D. Coord. Chem. Rev. 1997, 165, 93-161.
    • (1995) Angew. Chem., Int. Ed. Engl. , vol.34 , pp. 713-745
    • Böhmer, V.1
  • 2
    • 0012694411 scopus 로고    scopus 로고
    • For reviews, see: (a) Böhmer, V. Angew. Chem., Int. Ed. Engl. 1995, 34, 713-745; (b) Ikeda, A.; Shinkai, S. Chem. Rev. 1997, 97, 1713-1734; (c) Weiser, C.; Dieleman, C. B.; Matt, D. Coord. Chem. Rev. 1997, 165, 93-161.
    • (1997) Chem. Rev. , vol.97 , pp. 1713-1734
    • Ikeda, A.1    Shinkai, S.2
  • 3
    • 0031256183 scopus 로고    scopus 로고
    • For reviews, see: (a) Böhmer, V. Angew. Chem., Int. Ed. Engl. 1995, 34, 713-745; (b) Ikeda, A.; Shinkai, S. Chem. Rev. 1997, 97, 1713-1734; (c) Weiser, C.; Dieleman, C. B.; Matt, D. Coord. Chem. Rev. 1997, 165, 93-161.
    • (1997) Coord. Chem. Rev. , vol.165 , pp. 93-161
    • Weiser, C.1    Dieleman, C.B.2    Matt, D.3
  • 12
    • 1842740801 scopus 로고    scopus 로고
    • For reviews, see: (a) Hartwig, J. F. Synlett 1997, 329-340; (b) Hartwig, J. F. Angew. Chem., Int. Ed. 1998, 37, 2046-2067; (c) Yang, B. H.; Buchwald, S. L. J. Organomet. Chem. 1999, 576, 125-146.
    • (1997) Synlett , pp. 329-340
    • Hartwig, J.F.1
  • 13
    • 0032541260 scopus 로고    scopus 로고
    • For reviews, see: (a) Hartwig, J. F. Synlett 1997, 329-340; (b) Hartwig, J. F. Angew. Chem., Int. Ed. 1998, 37, 2046-2067; (c) Yang, B. H.; Buchwald, S. L. J. Organomet. Chem. 1999, 576, 125-146.
    • (1998) Angew. Chem., Int. Ed. , vol.37 , pp. 2046-2067
    • Hartwig, J.F.1
  • 14
    • 0008165462 scopus 로고    scopus 로고
    • For reviews, see: (a) Hartwig, J. F. Synlett 1997, 329-340; (b) Hartwig, J. F. Angew. Chem., Int. Ed. 1998, 37, 2046-2067; (c) Yang, B. H.; Buchwald, S. L. J. Organomet. Chem. 1999, 576, 125-146.
    • (1999) J. Organomet. Chem. , vol.576 , pp. 125-146
    • Yang, B.H.1    Buchwald, S.L.2
  • 23
    • 0010733407 scopus 로고    scopus 로고
    • note
    • 3): δ 156.0, 138.2, 107.0, 36.1.
  • 24
    • 0010733408 scopus 로고    scopus 로고
    • Formation of linear oligomers including acyclic trimer was also observed by HPLC and size exclusion chromatography.
    • Formation of linear oligomers including acyclic trimer was also observed by HPLC and size exclusion chromatography.
  • 26
    • 0010733381 scopus 로고    scopus 로고
    • -1, T=296 K, F(000)=672. A total of 7645 reflections were measured, 7641 unique. The structure was solved by direct method (SIR-92) and expanded by using Fourier techniques. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were included but not refined. The final cycle of full-matrix least squares refinement was based on 2215 observed reflections (I>3σ(I), 433 variable parameters) with factors of R=0.056, Rw=0.078, GOF=1.08.
    • -1, T=296 K, F(000)=672. A total of 7645 reflections were measured, 7641 unique. The structure was solved by direct method (SIR-92) and expanded by using Fourier techniques. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were included but not refined. The final cycle of full-matrix least squares refinement was based on 2215 observed reflections (I>3σ(I), 433 variable parameters) with factors of R=0.056, Rw=0.078, GOF=1.08.
  • 29
    • 0010692656 scopus 로고    scopus 로고
    • -1, T=296 K, F(000)=1472. A total of 2988 reflections were measured, 2886 unique. The structure was solved by direct methods (SAPI-90) and expanded by using Fourier techniques. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were included but not refined. The final cycle of full-matrix least squares refinement was based on 2191 observed reflections (I>3σ(I), 183 variable parameters) with factors of R=0.110, Rw=0.223, GOF=1.54.
    • -1, T=296 K, F(000)=1472. A total of 2988 reflections were measured, 2886 unique. The structure was solved by direct methods (SAPI-90) and expanded by using Fourier techniques. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were included but not refined. The final cycle of full-matrix least squares refinement was based on 2191 observed reflections (I>3σ(I), 183 variable parameters) with factors of R=0.110, Rw=0.223, GOF=1.54.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.