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8, 25 °C): δ 8.69 (s, 2 D, py-2), 7.59 (s, 1 D, py-4), 7.21 (s, 2 D, py-3). The pyridyl resonances were not resolved separately from the pyridine resonances.
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21
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33644553651
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1H NMR spectroscopy.
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23
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33644506312
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-, which contains an n-pentoxide group derived from the ring-opening of THF rather than the expected Nd methyl monocation (see ref 4b).
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25
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37049097715
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