Determination of total mercury in crude oil by combustion Cold Vapor Atomic Absorption Spectrometry (CVAAS)

ASTM Special Technical Publication

Volumn , Issue 1468, 2005, Pages 196-206

  Fox, Brian S ^a   Mason, Kelly John ^b   McElroy, Frank C ^b  

^a EXXONMOBIL UPSTREAM RESEARCH COMPANY   (United States)

^b ExxonMobil Research and Engineering   (United States)

Author keywords

Combustion CVAAS; Crude oil; Mercury

Indexed keywords

COAL; COMBUSTION; ELECTRIC POWER GENERATION; MERCURY (METAL); SPECTROMETRY;

ATMOSPHERIC MERCURY; COLD VAPOR ATOMIC ABSORPTION SPECTROMETRY (CVAAS); COMBUSTION CVAAS;

CRUDE PETROLEUM;

EID: 32944469755     PISSN: 00660558     EISSN: None     Source Type: Conference Proceeding    
DOI: 10.1520/stp12004s     Document Type: Conference Paper

References (13)

1. Edmonds, R., Moorwood, A. S., and Szczepanski, R., "Mercury Partitioning in Natural Gases and Condensates," Paper Presented to the GPA European Chapter Meeting, London, March 21, 1996.
2. Weise, E. and Watson, T., "Mercury in Many Lakes, Rivers," USA Today, Wednesday, August 25, 2004, p. 1.
3. Raines, B., "Mercury Testing Planned in Gulf," Mobile Register, Friday, March 22, 2002, p. 4A.
4. Wilhelm, S. M. and Bloom, N., "Review - Mercury in Petroleum," Fuel Processing Technology, Vol. 63, 2000, pp. 1-27.
5. Microwave Enhanced Chemistry, Kingston, H. M. and Haswell, S. J., Eds., American Chemical Society, 1997, pp. 380-381.
6. Bloom, N. S., "Analysis and Stability of Mercury Speciation in Petroleum Hydrocarbons," Fresnius J. Anal Chem, 2000, Vol. 366, pp. 438-443.
7. Liang, L., Lazoff, S., Horvat, M., Swain, E., and Gilkeson, J., "Determination of Mercury in Crude Oil by In-Situ Thermal Decomposition Using a Simple Lab Built System," Fresnius J. Anal Chem, 2000, Vol. 367, pp. 8-11.
8. US EPA Method 7473 - Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrometry.
9. Mercury Application Note #6 Rev. 01/20/04 - "Determination of Mercury in Crude Oil Using A Direct Mercury Analyzer," Milestone Incorporated, Monroe, CT 06468.
10. Total Mercury and Mercury Species in Liquid Hydrocarbons, UOP Method 938-00, UOP LLC, Des Plains, IL, 2004.
11. Instruction Manual for SP-3D, Nippon Instruments Corporation, Takatuki-shi, Osaka, Japan.
12. Anderson, R. L., Practical Statistics for Analytical Chemists, Van Nostrand Reinhold Company Inc., 1987, p. 299.
13. Teleconference with Dr. S. Mark Wilhelm.