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Volumn 45, Issue 3, 2006, Pages 949-951

Synthesis, characterization, and x-ray crystal structure of a gallium monohydroxide and a hetero-bimetallic gallium zirconium oxide

Author keywords

[No Author keywords available]

Indexed keywords

GALLIUM; HYDROXIDE; ORGANOMETALLIC COMPOUND; ZIRCONIUM; ZIRCONIUM OXIDE;

EID: 32544433674     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic051769l     Document Type: Article
Times cited : (47)

References (37)
  • 34
    • 32544456815 scopus 로고    scopus 로고
    • note
    • 2), -0.12 (s, 3 H, ZrMe), -0.32 (s, 3 H, GaMe).
  • 35
    • 32544440662 scopus 로고    scopus 로고
    • note
    • 22 All of the C-H hydrogen atoms except H(3A) were included in geometrically idealized positions and refined with the riding model. Localization of the H(3A) hydrogen from the electron density map in both structures proved to be more accurate than its fixing in the idealized position and led to lowering of the R1 and wR2 values. The hydrogen atom from the OH in 2 was localized from the difference electron density map and refined isotropically. (d) Compound 3 crystallizes as a pseudomerohedral twin emulating orthorhombic crystal system. The twin law was determined as - 1000 - 10001, and the ratio of the domains was refined as 0.33/0.67.
  • 36
    • 84943920736 scopus 로고
    • SHELXS-90, Program for Structure Solution
    • Sheldrick, G. M. SHELXS-90, Program for Structure Solution. Acta Crytallogr., Sect. A 1990, 46, 467-473.
    • (1990) Acta Crytallogr., Sect. A , vol.46 , pp. 467-473
    • Sheldrick, G.M.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.