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-1, KBr pellet): 1634(s), 1604(vs), 1554(m), 1513(m), 1473(s), 1447(m), 1438(m),1337(s), 1311(w), 1263(m), 1197(m), 1172(m), 1153(m), 1129(m), 1085(m), 1027(vs), 847(s) 774(s), 732(w), 597(m)
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1 was 0.0588 for I>2σ(I) and 0.1416 for all 3520 reflections. All absorption corrections were performed using the SADABS program. The structure solution and refinement were carried out using SHELXTL programs. Details of the crystallographic data have been deposited at the Cambridge crystallographic Data Center (CCDC 232843)
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