Search of structure and ligands exchange for palladium(II) complexes with N-allylimidazole; X-ray and solid-state/solution NMR studies

Journal of Organometallic Chemistry

Volumn 691, Issue 5, 2006, Pages 869-878

  Kurdziel, Krystyna ^a   Olejniczak, Sebastian ^b   Okruszek, Andrzej ^b,c   Głowiak, Tadeusz ^d   Kruszyński, Rafał ^c   Materazzi, Stefano ^e   Potrzebowski, Marek J ^b  

^a JAN KOCHANOWSKI UNIVERSITY   (Poland)

^b CENTRE OF MOLECULAR AND MACROMOLECULAR STUDIES   (Poland)

^c LODZ UNIVERSITY OF TECHNOLOGY   (Poland)

^d UNIVERSITY OF WROC AW   (Poland)

^e SAPIENZA UNIVERSITY OF ROME   (Italy)

Author keywords

2D NMR; 13C solid state NMR; DFT calculations; Metal complexes; NMR shielding

Indexed keywords

COMPLEXATION; CRYSTAL STRUCTURE; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; REACTION KINETICS; SINGLE CRYSTALS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

2D NMR; 13C SOLID-STATE NMR; DFT CALCULATIONS; METAL COMPLEXES; NMR SHIELDING;

PALLADIUM COMPOUNDS;

EID: 31644443871     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jorganchem.2005.10.045     Document Type: Article

References (36)

1. A. Togni, and L.M. Venanzi Angew. Chem., Int. Ed. 33 1994 497 526
2. G.A. Grasa, A.C. Hillier, and S.P. Nolan Org. Lett. 3 2001 1077 1080
3. A.S. Abu-Surrah, M. Kettunen, K. Lappalainen, U. Piironen, M. Klinga, and M. Leskelä Polyhedron 21 2002 27 31
4. C. Mazet, and L.H. Gade Organometallics 20 2001 4144 4166
5. M.R. Buchmeiser, Th. Schareina, R. Kempe, and K. Wurst J. Organomet. Chem. 634/1 2001 39 46
6. J. Silberg, T. Schareina, R. Kempe, K. Wurst, and M.R. Buchmeiser J. Organomet. Chem. 622 2001 6 18
7. M.R. Buchmeiser, and K. Wurst J. Am. Chem. Soc. 121 1999 11101 11107
8. D.J. Nielsen, K.J. Cavell, B.W. Skelton, and A.H. White Organometallics 20 2001 995 1000
9. M.C. Done, T. Ruether, K.J. Cavell, M. Kilner, E.J. Peacock, N. Braussaud, B.W. Skelton, and A.H. White J. Organometal. Chem. 607 2000 78 92
10. K.R. Reddy, and G.G. Krishna Tetrahedron Lett. 46 2005 661 663
11. C.J. Mathews, P.J. Smith, and T. Welton J. Mol. Catal. Chem. 206 2003 77 82
12. F.E. Hahn, B. Heidrich, T. Lugger, and T. Pape Z. Naturforsch. B 59 2004 1519 1523
13. STOE & Cie, X-RED, Version 1.18. STOE & Cie GmbH, Darmstadt, Germany, 1999.
14. G.M. Sheldrick Acta Crystallogr. A46 1990 467 473 and references cited therein
15. G.M. Sheldrick shelx97, Program for the Solution of Crystal Structures 1997 University of Göttingen Germany
16. G.M. Sheldrick, shelxtl: Release 4.1 for Siemens Crystallographic Research Systems, 1990.
17. S. Berger, and S. Braun 200 and More NMR Experiments, A Practical Course 2004 Wiley-VCH Verlag-GmbH CoKGaA, Weinheim
18. G. Metz, X. Wu, and S.O. Smith J. Magn. Reson. A 110 1994 219 227
19. A.E. Bennet, C.M. Rienstra, M. Auger, K.V. Lakashmi, and R.G. Griffin J. Chem. Phys. 103 1995 6951 6958
20. win-nmr, Bruker-Franzen Analytik GmbH, Version 6.0, Bremen, Germany, 1993.
21. O.N. Antzutkin, S.C. Shekar, and M.H. Levitt J. Magn. Reson. 115 1995 7 18
22. O.N. Antzutkin, Y.K. Lee, and M.H. Levitt J. Magn. Reson. 135 1998 144 152
23. O.N. Antzutkin Prog. Nucl. Mag. Res. Sp. 35 1999 203 266
24. M.J. Frisch, G.W. Trucks, H.B. Schlegel, G.E. Scuseria, M.A. Robb, J.R. Cheeseman, V.G. Zakrzewski, J.A. Montgomery Jr., R.E. Stratmann, J.C. Burant, S. Dapprich, J.M. Millam, A.D. Daniels, K.N. Kudin, M.C. Strain, O. Farkas, J. Tomasi, V. Barone, M. Cossi, R. Cammi, B. Mennucci, C. Pomelli, C. Adamo, S. Clifford, J. Ochterski, G.A. Petersson, P.Y. Ayala, Q. Cui, K. Morokuma, D.K. Malick, A.D. Rabuck, K. Raghavachari, J.B. Foresman, J. Cioslowski, J.V. Ortiz, B.B. Stefanov, G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. Gomperts, R.L. Martin, D.J. Fox, T. Keith, M.A. Al-Laham, C.Y. Peng, A. Nanayakkara, C. Gonzalez, M. Challacombe, P.M.W. Gill, B. Johnson, W. Chen, M.W. Wong, J.L. Andres, C. Gonzalez, M. Head-Gordon, E.S. Replogle, and J.A. Pople gaussian 98, Revision A.6 1998 Gaussian, Inc. Pittsburgh, PA
25. The refcodes of analysed compounds are available from authors on request.
26. K. Kurdziel, and T. Głowiak Pol. J. Chem. 72 1998 2181 2188
27. T. Głowiak, and K. Kurdziel J. Mol. Struct. 516 2000 1 5
28. K. Kurdziel, and T. Głowiak Polyhedron 19 2000 2183 2188
29. A. Bielecki, A.C. Kolbert, and M.H. Levitt Chem. Phys. Lett. 155 1989 341 346
30. K.W. Zilm D.M. Grant R.K. Harris Spectral Editing Techniques: Hydrocarbon Solids in Encyclopedia of NMR vol. 7 1996 Wiley Chichester 4498 4503
31. W.S. Veeman Prog. Nucl. Mag. Res. Sp. 16 1984 193 235
32. J. Herzfeld, and A. Berger J. Chem. Phys. 73 1980 6021 6030
33. G. Jeschke, and G. Grossmann J. Magn. Reson. A 103 1993 323 328
34. D.M. Grant, J.C. Facelli, D.W. Alderman, and M.H. Sherwood J.A. Tossell Nuclear Magnetic Shielding and Molecular Structure 1993 Kluwer, Academic Publishers Dordrecht 367 384
35. M. Buhl, M. Kaupp, O.L. Malkina, and V.G. Malkin J. Comput. Chem. 20 1999 91 105
36. See Supplementary materials.