X-ray crystal structure of 3β,22-dihydroxy-23,24-dinorchol-4-ene

Journal of Chemical Research

Volumn , Issue 5, 2004, Pages 372-373

  Cox, Philip J ^a   Nahar, Lutfun ^a   Turner, Alan B ^b  

^a ROBERT GORDON UNIVERSITY   (United Kingdom)

^b UNIVERSITY OF ABERDEEN   (United Kingdom)

Author keywords

Steroids; X ray crystallography

Indexed keywords

3 OXO 23,24 DINORCHOL 4 EN 22 AL; 3BETA,22 DIHYDROXY 23,24 DINORCHOL 4 ENE; STEROID; UNCLASSIFIED DRUG;

ARTICLE; CHIRALITY; CONFORMATION; CRYSTAL STRUCTURE; HYDROGEN BOND; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 3142545182     PISSN: 03082342     EISSN: None     Source Type: Journal    
DOI: 10.3184/0308234041639809     Document Type: Article

References (9)

1. L. Nahar and A.B. Turner, Tetrahedron, 2003, 59, 8623.
2. W.L. Duax, C.M. Weeks and D.C. Rohrer, Topics in Stereochemistry, E.L. Eliel and N. Allinger (eds.), Vol. 9, 1976, p. 271.
3. P.J. Cox, L. Nahar, S.D. Sarker and A.B. Turner, J. Chem. Res. (S) 2004, 192.
4. Z. Otwinowski and W. Minor, Processing of X-ray Diffraction Data Collected in Oscillation Mode, Methods in Enzymology, Vol. 276: Macromolecular Crystallography, part A, p. 307-326. Carter, C. W. Jr. and Sweet, R. M., eds., Academic Press, 1997.
5. R. Hooft. COLLECT Data collection software. Nonius B.V., Delft, The Netherlands, 1998.
6. A. Altomare, M.C. Burla, M. Camalli, G.L. Cascarano, C. Giacovazzo, A. Guagliardi, A.G.G. Molitemi, G. Polidori and R. Spagna, J. Appl. Cryst., 1999, 32, 115.
7. G.M. Sheldrick. SHELX97-2. Program for the Refinement of Crystal Structures. Univ. of Göttingen, Germany, 1998.
8. A.L. Spek, J. Appl. Cryst., 2003, 36, 7.
9. I. Vincze, C. Somali, G. Scheider, G. Dombi and A. Kalman, Liebigs Ann. Chem., 1987, 6, 499.