Synthesis and X-ray crystal structure of 3-oxo-23, 24-dinorchol-4-ene-22-cyanohydrin

Journal of Chemical Research

Volumn , Issue 3, 2004, Pages 192-193

  Cox, Philip J ^a   Nahar, Lutfun ^b   Sarker, Satyajit D ^a   Turner, Alan B ^b  

^a ROBERT GORDON UNIVERSITY   (United Kingdom)

^b UNIVERSITY OF ABERDEEN   (United Kingdom)

Author keywords

Epimers; Steroids; X ray crystallography

Indexed keywords

3 OXO 23,24 DINORCHOL 4 ENE 22 AL; 3 OXO 23,24 DINORCHOL 4 ENE 22 CYANOHYDRIN; CYANOHYDRIN; STEROID; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; EPIMER; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 2942586800     PISSN: 03082342     EISSN: None     Source Type: Journal    
DOI: 10.3184/0308234041640618     Document Type: Article

References (8)

1. F.H. Allen, Acta Cryst., 2002, B58, 380.
2. W.L. Duax, C.M. Weeks and D.C. Rohrer, Topics in Stereochemistry, E.L. Eliel and N. Allinger (eds), Vol. 9, 1976, p. 271.
3. F.W. Heyl and M.E. Herr, J. Am. Chem. Soc., 1950, 72, 2617.
4. Z. Otwinowski and W. Minor, Processing of X-ray Diffraction Data Collected in Oscillation Mode, Methods in Enzymology, Vol. 276: Macromolecular Crystallography, part A, pp.307-326. Carter, C.W. Jr. and Sweet, R.M., (eds), Academic Press, 1997.
5. R. Hooft. COLLECT Data collection software. Nonius B.V., Delft, The Netherlands, 1998.
6. A. Altomare, M.C. Burla, M. Camalli, G.L. Cascarano, C. Giacovazzo, A. Guagliardi, A.G.G. Moliterni, G. Polidori and R. Spagna, J. Appl. Cryst., 1999, 32, 115.
7. G.M. Sheldrick. SHELX97-2. Program for the Refinement of Crystal Structures. Univ. of Göttingen, Germany, 1998.
8. A.L. Spek. PLATON. Program for geometrical analysis of X-ray molecular structure. Univ. of Utrecht, The Netherlands, 2001. Version 101201.