The graphite arc-discharge in the presence of CCl4: Chlorinated carbon clusters in relation with fullerenes formation

Carbon

Volumn 42, Issue 10, 2004, Pages 1959-1963

  Gao, Fei ^a   Xie, Su Yuan ^a,c   Ma, Zhi Jie ^a   Feng, Yu Qi ^b   Huang, Rong Bin ^a   Zheng, Lan Sun ^a  

^a XIAMEN UNIVERSITY   (China)

^b WUHAN UNIVERSITY   (China)

^c CLEMSON UNIVERSITY   (United States)

Author keywords

A. Fullerene; B. Arc discharge; C. Mass spectrometry; Carbon clusters

Indexed keywords

BYPRODUCTS; CARBON NANOTUBES; CARBON TETRACHLORIDE; FULLERENES; GROWTH KINETICS; HELIUM; MASS SPECTROMETRY; PARTIAL PRESSURE; POLYCYCLIC AROMATIC HYDROCARBONS; REACTION KINETICS;

ARC DISCHARGES; CARBON CLUSTERS; FORMATION MECHANISM; REACTION MEDIA;

GRAPHITE;

EID: 3042852626     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2004.03.028     Document Type: Article

References (30)

1. 60: a new form of carbon. Nature. 347:1990;354-358.
2. Smalley R.E. Self-assembly of the fullerenes. Acc. Chem. Res. 25:1992;98-105.
3. Goroff N.S. Mechanism of fullerene formation. Acc. Chem. Res. 29:1996;77-83.
4. Rabideau P.W., Sygula A. Buckybowls: polynuclear aromatic hydrocarbons related to the buckminsterfullerene surface. Acc. Chem. Res. 29:1996;235-242.
5. 30 polyarene. Science. 294:2001;828-831.
6. von Helden G., Gotts N.G., Bowers M.T. Experimental-evidence for the formation of fullerenes by collisional heating of carbon rings in the gas phase. Nature. 363:1993;60-63.
7. McElvany S.W., Ross M.M., Goroff N.S., Diederich F. Cyclocarbon coalescence - mechanisms for tailor-made fullerene formation. Science. 259:1993;1594-1596.
8. Schwarz H. The mechanism of fullerene formation. Angew Chem. Int. Ed. 32:1993;1412-1415.
9. 12. Angew Chem. Int. Ed. 37:1998;1226-1229.
10. Alekseyev N.I., Dyuzhev G.A. Fullerene formation in an arc dishcharge. Carbon. 41:2003;1343-1348.
11. Churilov G.N., Fedorov A.S., Novikov P.V. Influence of electron concentration and temperature on fullerene formation in a carbon plasma. Carbon. 41:2003;173-178.
12. Churilov G.N., Novikov P.V., Tarabanko V.E., Lopatin V.A., Vnukova N.G., Bulina N.V. On the mechanism of fullerene formation in a carbon plasma. Carbon. 40:2002;891-896.
13. Grösser T., Hirsch A. Dicyanopolyynes: formation of new rod-shaped molecules in a carbon plasma. Angew Chem. Int. Ed. Engl. 32:1993;1340-1342.
14. Heath J.R., Zhang Q., O'Brien S.C., Curl R.F., Kroto H.W., Smalley R.E. The formation of long carbon chain molecules during laser vaporization of graphite. J. Am. Chem. Soc. 109:1987;359-363.
15. Chang T.M., Naim A., Ahmed S.N., Goodloe G., Shevlin P.B. On the mechanism of formation. trapping of some possible intermediates. J. Am. Chem. Soc. 114:1992;7603-7604.
16. Xie S.Y., Huang R.B., Deng S.L., Yu L.J., Zheng L.S. Synthesis, separation, and characterization of fullerenes and their chlorinated fragments in the glow discharge reaction of chloroform. J. Phys. Chem. B. 105:2001;1734-1738.
17. Xie S.Y., Huang R.B., Yu L.J., Ding J., Zheng L.S. Microwave synthesis of fullerenes from chloroform. Appl. Phys. Lett. 75:1999;2764-2766.
18. 70) by coupling high-performance liquid chromatography with ultraviolet absorption spectroscopy and atmospheric pressure chemical ionization mass spectrometry. J. Chromatogr. A. 932:2001;43-53.
19. Wan J.D., Feng Y.Q., Hu Y.L., Da S.L., Wang Z.H. Preparation and evaluation of 2,4,6-trinitrophenol-modified zirconia-alumina for high performance liquid chromatography and its application in the separation of fullerenes. Chem. J. Chin. U. 23:2002;1259-1263.
20. 70. Anal. Sci. 17:2001;a321-a324.
21. Huang R.B., Huang W.J., Wang Y.H., Tang Z.C., Zheng L.S. Preparation of decachlorocorannulene and other perchlorinated fragments of fullerenes by electrical discharge in liquid chloroform. J. Am. Chem. Soc. 119:1997;5954-5955.
22. Alexakis Th., Tsantrizos P.G., Tsantrizos Y.S., Meunier J.L. Synthesis of fullerenes via the thermal plasma dissociation of hydrocarbons. Appl. Phys. Lett. 70:1997;2102-2104.
23. 4. J. Phys. D: Appl. Phys. 30:1997;2403-2410.
24. 4. PhD thesis, McGill University, Canada, 1997.
25. 266. J. Am. Chem. Soc. 113:1991;7499-7503.
26. 60 by plasma discharge in a modified round-bottomed flask. Key parameters for yield optimization and purification. J. Org. Chem. 57:1992;6932-6936.
27. Weston A., Murthy M. Synthesis of fullerenes: an effort to optimize process parameters. Carbon. 10:1996;1267-1274.
28. 4 on fullerene yield in the graphite arc-discharge reaction. Chem. Commun. 2003;2676-2677.
29. Tang Z.C., Huang R.B., Chen H., Zheng L.S. Laser productions of fullerene ions promoted by additive compounds in carbon targets. J. Phys. Chem. A. 102:1998;9993-9998.
30. 10. Science 2004: in press.