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3042816368
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note
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Compound 41 was synthesized by Sonogashira coupling of 2-bromoiodobenzene and phenylacetylene and further application of our standard protocol for obtaining the corresponding boronate ester derivative.
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3042855730
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note
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The addition of fluoride may also promote the formation of a catalytically active fluororhodium(I) intermediate.
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36
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0000884858
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(a) For preparation of t-Bu-amphos-Cl 3 and an account of its efficiency for Pd-catalyzed Suzuki couplings in aqueous media, see: Shaughnessy, K. H.; Booth, R. S. Org. Lett. 2001, 3, 2757.
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