Strong intramolecular secondary Si⋯N bonds in trifluorosilylhydrazines

Chemistry - A European Journal

Volumn 10, Issue 12, 2004, Pages 3033-3042

  Vojinović, Krunoslav ^a   McLachlan, Lorna J ^b   Hinchley, Sarah L ^b   Rankin, David W H ^b   Mitzel, Norbert W ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

^b UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

Crystal structure; Donor bonds; Electron diffraction; Hydrazines; Silicon

Indexed keywords

CHEMICAL BONDS; MASS SPECTROMETRY; NITROGEN; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SUBSTITUTION REACTIONS; X RAY CRYSTALLOGRAPHY;

FREE MOLECULES; SUBSTITUENTS;

ORGANIC COMPOUNDS;

FLUORINE DERIVATIVE; HYDRAZINE DERIVATIVE; NITROGEN; SILICON; SILICON DERIVATIVE; TRIFLUOROSILYLHYDRAZINE DERIVATIVE; UNCLASSIFIED DRUG;

AB INITIO CALCULATION; ARTICLE; ATOM; CHEMICAL BOND; CHEMICAL REACTION; CRYSTAL STRUCTURE; ELECTRON DIFFRACTION; GAS; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; MOLECULAR INTERACTION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 3042740819     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/chem.200400069     Document Type: Article

References (41)

1. a) R. N. Haszeldine, J. C. Young, J. Chem. Soc. 1959, 394;
2. b) H. Beckers, H. Bürger, J. Organomet. Chem. 1990, 385, 207.
3. Y. H. Chang, F.-T. Chiu, G. Zon, J. Org. Chem. 1981, 46, 352.
4. N. F. Lazareva, V. P. Baryshok, M. G. Voronkov, Russ. Chem. Bull. 1995, 104, 374.
5. Y. Hamada, S. Mori, Proceedings of the 29th Organosilicon Symposium, March 1996, Evanston, USA.
6. A collection of patent literature references can be found in: M. G. Voronkov, E. A. Maletina, V. K. Roman, Heterosiloxanes, Vol. 2: Derivates of Nitrogen and Phosphorus, Harwood, Chur, Switzerland 1991.
7. S. Schmatz, C. Ebker, T. Labahn, H. Stoll, U. Klingebiel, Organometallics 2003, 22, 490.
8. a) R. West, P. Novakovski, J. Am. Chem. Soc. 1976, 98, 5616;
9. b) R. West, P. Novakovski, P. Boudjouk, J. Am. Chem. Soc. 1976, 98, 5620;
10. c) R. West, P. Boudjouk, Intra-Sci. Chem. Rep., 1973, 765.
11. a) S. Schmatz, F. Diedrich, C. Ebker, U. Klingebiel, Eur. J. Inorg. Chem. 2002, 876;
12. b) R. Wolfgramm, T. Müller, U. Klingebiel, Organometallics, 1998, 17, 3222.
13. N. W. Mitzel, U. Losehand, Angew. Chem. 1997, 109, 2897; Angew. Chem. Int. Ed. Engl. 1997, 36, 2807.
14. N. W. Mitzel, U. Losehand, Angew. Chem. 1997, 109, 2897; Angew. Chem. Int. Ed. Engl. 1997, 36, 2807.
15. N. W. Mitzel, U. Losehand, J. Am. Chem. Soc. 1998, 120, 7320.
16. N. W. Mitzel, U. Losehand, A. Wu, D. Cremer, D. W. H. Rankin, J. Am. Chem. Soc. 2000, 122, 4471.
17. K.R. Leopold, M. Canagaratna, J.A. Phillips, Acc. Chem. Res. 1997, 30, 57.
18. N. W. Mitzel, Chem. Eur. J. 1998, 4, 692.
19. a) E. Gellermann, U. Klingebiel, H. Noltemeyer, S. Schmatz, J. Am. Chem. Soc. 2001, 123, 382;
20. b) U. Klingebiel, H. Hluchy, A. Meller, Chem. Ber. 1978, 111, 906;
21. c) E. Gellermann, U. Klingebiel, T. Pape, F. D. Antonia, T. Schneider, S. Schmatz, Z. Anorg. Allg. Chem. 2001, 627, 2581;
22. d) H. Witte-Abel, U. Klingebiel, M. Schaefer, Z. Anorg. Allg. Chem. 1998, 624, 271;
23. e) K. Bode, U. Klingebiel, H. Witte-Abel, M. Sluth, M. Noltemeyer, R. Herbst-Irmer, M. Schäfer, W. Shomaky, Phosphorus Sulfur Silicon Relat. Elem. 1996, 108, 121;
24. f) K. Kipping, C. Drost, U. Klingebiel, M. Noltemeyer, Z. Anorg. Allg. Chem. 1996, 622, 1215.
25. N. W. Mitzel, D. W. H. Rankin, J. Chem. Soc. Dalton Trans. 2003, 3650.
26. N. W. Mitzel, B. A. Smart, A. J. Blake, S. Parsons, D. W. H. Rankin, J. Chem. Soc. Dalton Trans. 1996, 2095.
27. M. Korth, S. Grimme, K. Vojinović, N. W. Mitzel, unpublished results.
28. W. S. Sheldrick, W. Wolfsberger, Z. Naturforsch. B 1977, 32, 22.
29. K. Vojinović, N. W. Mitzel, D. W. H. Rankin, unpublished results.
30. N. W. Mitzel, U. Losehand, A. Richardson, Organometallics 1999, 18, 2610.
31. U. Losehand, Thesis, Technische Universität München, 1999.
32. a) R. T. Beltrami, E. R. Bissell, J. Am. Chem. Soc. 1956, 78, 2467;
33. b) J. B. Claas, J. G. Aston, T. S. Oakwood, J. Am. Chem. Soc. 1953, 75, 2937.
34. U. Wannagat, F. Höfler, Monatsh. Chem. 1966, 97, 976.
35. N. Wiberg, M. Veith, Chem. Ber. 1971, 104, 3191.
36. SCALEPACK: Z. Otwinowski, W. Minor, Methods Enzymol. 1997, 276, 307.
37. SHELXTL-PC 4.1 Siemens Analytical X-Ray Instruments Inc. 1990.
38. C. M. Huntley, G. S. Laurenson, D. W. H. Rankin, J. Chem. Soc. Dalton Trans. 1980, 945.
39. J. R. Lewis, P. T. Brain, D. W. H. Rankin, Spectrum 1997, 15, 7.
40. A. S. F. Boyd, G. Laurenson, D. W. H. Rankin, J. Mol. Struct. 1981, 71, 217.
41. A. W. Ross, M. Fink, R. Hilderbrandt, International Tables for X-Ray Crystallography, Vol. C, (Ed.: A. J. C. Wilson), Kluwer, Dodrecht, Boston, 1992, p. 245.