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85194972063
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Crystals were obtained from acetone. The intensities were measured on a Siemens SMART CCD diffractometer. Data collection and cell refinement are listed in the text. The structure was solved by direct methods with SHELX-97 [19]. The refinement was done with SHELXL-97 [20]. Crystallographic data for the structural analyses have been deposited with the Cambridge Crystallographic Data Centre, CCDC No. 268977 for 12f. Copies of the data can be obtained, free of charge, from CCDC, 12 Union Road, Cambridge, CB2 1EZ. UK [fax: +44(1233)336033; e-mail: deposit@ccdc.cam.ac.uk; internet: http://www.ccdc.cam.ac.uk].
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