메뉴 건너뛰기




Volumn 29, Issue 1-3, 2006, Pages 119-124

A combined 17O RAPT and MQ-MAS NMR study of L-leucine

Author keywords

17O; Amino acids; MQ MAS; RAPT

Indexed keywords

AMINO ACIDS; COMPUTER SIMULATION; COUPLED CIRCUITS; NATURAL FREQUENCIES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PARAMETER ESTIMATION;

EID: 29144491720     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ssnmr.2005.10.007     Document Type: Article
Times cited : (15)

References (30)
  • 1
    • 4544264076 scopus 로고    scopus 로고
    • A review of oxygen-17 solid-state NMR of organic materials - Towards biological applications
    • V. Lemaitre, M.E. Smith, and A. Watts A review of oxygen-17 solid-state NMR of organic materials - towards biological applications Solid State Nucl. Magn. Reson. 26 3-4 2004 215 235
    • (2004) Solid State Nucl. Magn. Reson. , vol.26 , Issue.34 , pp. 215-235
    • Lemaitre, V.1    Smith, M.E.2    Watts, A.3
  • 2
    • 0001435784 scopus 로고    scopus 로고
    • 17O NMR chemical shifts and quadrupole coupling constants in solid poly(l-alanine)s determined using a high-speed MAS technique
    • K. Yamauchi, S. Kuroki, I. Ando, T. Ozaki, and A. Shoji O 17 NMR chemical shifts and quadrupole coupling constants in solid poly(l-alanine)s determined using a high-speed MAS technique Chem. Phys. Lett. 302 1999 331 336
    • (1999) Chem. Phys. Lett. , vol.302 , pp. 331-336
    • Yamauchi, K.1    Kuroki, S.2    Ando, I.3    Ozaki, T.4    Shoji, A.5
  • 3
    • 0037045263 scopus 로고    scopus 로고
    • 17O NMR studies of polyglycines and their hydrogen-bonded structures
    • K. Yamauchi, S. Kuroki, and I. Ando High-resolution solid-state O 17 NMR studies of polyglycines and their hydrogen-bonded structures J. Mol. Struct. 602-603 2002 171 175
    • (2002) J. Mol. Struct. , vol.602-603 , pp. 171-175
    • Yamauchi, K.1    Kuroki, S.2    Ando, I.3
  • 4
    • 0035913713 scopus 로고    scopus 로고
    • 17O multiple quantum magic-angle spinning NMR of organic solids
    • G. Wu, and S. Dong Two-dimensional O 17 multiple quantum magic-angle spinning NMR of organic solids J. Am. Chem. Soc. 123 37 2001 9119 9125
    • (2001) J. Am. Chem. Soc. , vol.123 , Issue.37 , pp. 9119-9125
    • Wu, G.1    Dong, S.2
  • 5
    • 0037470686 scopus 로고    scopus 로고
    • New insights into the bonding arrangements of l- and d- glutamates from solid state O-17 NMR
    • V. Lemaitre, K.J. Pike, A. Watts, T. Anupold, A. Samoson, M.E. Smith, and R. Dupree New insights into the bonding arrangements of l- and d- glutamates from solid state O-17 NMR Chem. Phys. Lett. 371 1-2 2003 91 97
    • (2003) Chem. Phys. Lett. , vol.371 , Issue.12 , pp. 91-97
    • Lemaitre, V.1    Pike, K.J.2    Watts, A.3    Anupold, T.4    Samoson, A.5    Smith, M.E.6    Dupree, R.7
  • 7
    • 9644273777 scopus 로고    scopus 로고
    • 17O NMR as a probe for structural studies of proteins in biomembranes
    • V. Lemaitre, R.R. Maurits, A.P. Howes, M.E. Smith, R. Dupree, and A. Watts Solid state O 17 NMR as a probe for structural studies of proteins in biomembranes J. Am. Chem. Soc. 126 47 2004 15320 15321
    • (2004) J. Am. Chem. Soc. , vol.126 , Issue.47 , pp. 15320-15321
    • Lemaitre, V.1    Maurits, R.R.2    Howes, A.P.3    Smith, M.E.4    Dupree, R.5    Watts, A.6
  • 8
    • 3242886145 scopus 로고    scopus 로고
    • Theoretical investigation of oxygen-17 NMR shielding and electric field gradients in glutamic acid polymorphs
    • J.R. Yates, C.J. Pickard, M.C. Payne, R. Dupree, M. Profeta, and F. Mauri Theoretical investigation of oxygen-17 NMR shielding and electric field gradients in glutamic acid polymorphs J. Phys. Chem. A 108 28 2004 6032 6037
    • (2004) J. Phys. Chem. A , vol.108 , Issue.28 , pp. 6032-6037
    • Yates, J.R.1    Pickard, C.J.2    Payne, M.C.3    Dupree, R.4    Profeta, M.5    Mauri, F.6
  • 9
    • 0037042272 scopus 로고    scopus 로고
    • A simple technique for determining nuclear quadrupole coupling constants with RAPT solid-state NMR spectroscopy
    • S. Prasad, H.T. Kwak, T. Clark, and P.J. Grandinetti A simple technique for determining nuclear quadrupole coupling constants with RAPT solid-state NMR spectroscopy J. Am. Chem. Soc. 124 18 2002 4964 4965
    • (2002) J. Am. Chem. Soc. , vol.124 , Issue.18 , pp. 4964-4965
    • Prasad, S.1    Kwak, H.T.2    Clark, T.3    Grandinetti, P.J.4
  • 10
    • 0042415778 scopus 로고    scopus 로고
    • Selective suppression and excitation of solid-state NMR resonances based on quadrupole coupling constants
    • H.T. Kwak, S. Prasad, T. Clark, and P.J. Grandinetti Selective suppression and excitation of solid-state NMR resonances based on quadrupole coupling constants J. Magn. Reson. 160 2 2003 107 113
    • (2003) J. Magn. Reson. , vol.160 , Issue.2 , pp. 107-113
    • Kwak, H.T.1    Prasad, S.2    Clark, T.3    Grandinetti, P.J.4
  • 11
    • 0042890463 scopus 로고    scopus 로고
    • Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers
    • H.T. Kwak, S. Prasad, T. Clark, and P.J. Grandinetti Enhancing sensitivity of quadrupolar nuclei in solid-state NMR with multiple rotor assisted population transfers Solid State Nucl. Magn. Reson. 24 2-3 2003 71 77
    • (2003) Solid State Nucl. Magn. Reson. , vol.24 , Issue.23 , pp. 71-77
    • Kwak, H.T.1    Prasad, S.2    Clark, T.3    Grandinetti, P.J.4
  • 14
    • 0034145865 scopus 로고    scopus 로고
    • Pure absorption-mode spectra using a modulated RF mixing period in MQMAS experiments
    • T. Vosegaard, P. Florian, P.J. Grandinetti, and D. Massiot Pure absorption-mode spectra using a modulated RF mixing period in MQMAS experiments J. Magn. Reson. 143 2000 217 222
    • (2000) J. Magn. Reson. , vol.143 , pp. 217-222
    • Vosegaard, T.1    Florian, P.2    Grandinetti, P.J.3    Massiot, D.4
  • 15
    • 0001421829 scopus 로고
    • Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR
    • L. Frydman, and J.S. Harwood Isotropic spectra of half-integer quadrupolar spins from bidimensional magic-angle spinning NMR J. Am. Chem. Soc. 117 1995 5367 5369
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 5367-5369
    • Frydman, L.1    Harwood, J.S.2
  • 16
    • 0002099140 scopus 로고    scopus 로고
    • Sensitivity enhancement of the MQ-MAS NMR experiment by fast amplitude modulation of the pulses
    • P.K. Madhu, A. Goldbourt, L. Frydman, and S. Vega Sensitivity enhancement of the MQ-MAS NMR experiment by fast amplitude modulation of the pulses Chem. Phys. Lett. 307 1999 41 47
    • (1999) Chem. Phys. Lett. , vol.307 , pp. 41-47
    • Madhu, P.K.1    Goldbourt, A.2    Frydman, L.3    Vega, S.4
  • 18
    • 36749113303 scopus 로고
    • Fictitious spin-1/2 operator formalism for multiple quantum NMR
    • S. Vega Fictitious spin- 1 2 operator formalism for multiple quantum NMR J. Chem. Phys. 68 1978 5518 5527
    • (1978) J. Chem. Phys. , vol.68 , pp. 5518-5527
    • Vega, S.1
  • 19
    • 0000462578 scopus 로고
    • Selective excitation and detection in multilevel spin systems: Application of single transition operators
    • A. Wokaun, and R.R. Ernst Selective excitation and detection in multilevel spin systems: application of single transition operators J. Chem. Phys. 67 1977 1752 1758
    • (1977) J. Chem. Phys. , vol.67 , pp. 1752-1758
    • Wokaun, A.1    Ernst, R.R.2
  • 20
    • 0003152304 scopus 로고    scopus 로고
    • Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning
    • Z. Yao, H.T. Kwak, D. Sakellariou, L. Emsley, and P.J. Grandinetti Sensitivity enhancement of the central transition NMR signal of quadrupolar nuclei under magic-angle spinning Chem. Phys. Lett. 327 1-2 2000 85 90
    • (2000) Chem. Phys. Lett. , vol.327 , Issue.12 , pp. 85-90
    • Yao, Z.1    Kwak, H.T.2    Sakellariou, D.3    Emsley, L.4    Grandinetti, P.J.5
  • 21
    • 0037413308 scopus 로고    scopus 로고
    • Modulation aided signal enhancement in the magic angle spinning NMR of spin-5/2 nuclei
    • P.K. Madhu, K.J. Pike, R. Dupree, M.H. Levitt, and M.E. Smith Modulation aided signal enhancement in the magic angle spinning NMR of spin- 5 2 nuclei Chem. Phys. Lett. 367 1-2 2003 150 156
    • (2003) Chem. Phys. Lett. , vol.367 , Issue.12 , pp. 150-156
    • Madhu, P.K.1    Pike, K.J.2    Dupree, R.3    Levitt, M.H.4    Smith, M.E.5
  • 22
    • 0035742228 scopus 로고    scopus 로고
    • Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer
    • H.T. Kwak, S. Prasad, Z. Yao, P.J. Grandinetti, J.R. Sachleben, and L. Emsley Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer J. Magn. Reson. 150 1 2001 71 80
    • (2001) J. Magn. Reson. , vol.150 , Issue.1 , pp. 71-80
    • Kwak, H.T.1    Prasad, S.2    Yao, Z.3    Grandinetti, P.J.4    Sachleben, J.R.5    Emsley, L.6
  • 23
    • 0036295243 scopus 로고    scopus 로고
    • Signal enhancement in the triple-quantum magic-angle spinning NMR of spins-3/2 in solids: The FAM-RIACT-FAM sequence
    • P.K. Madhu, and M.H. Levitt Signal enhancement in the triple-quantum magic-angle spinning NMR of spins- 3 2 in solids: the FAM-RIACT-FAM sequence J. Magn. Reson. 155 1 2002 150 155
    • (2002) J. Magn. Reson. , vol.155 , Issue.1 , pp. 150-155
    • Madhu, P.K.1    Levitt, M.H.2
  • 24
    • 0036307503 scopus 로고    scopus 로고
    • Efficient triple-quantum excitation in modified RIACT MQMAS NMR for i = 3/2 nuclei
    • K.H. Lim, T. Charpentier, and A. Pines Efficient triple-quantum excitation in modified RIACT MQMAS NMR for I = 3 2 nuclei J. Magn. Reson. 154 2 2002 196 204
    • (2002) J. Magn. Reson. , vol.154 , Issue.2 , pp. 196-204
    • Lim, K.H.1    Charpentier, T.2    Pines, A.3
  • 25
    • 0000539519 scopus 로고
    • Satellite transition spectroscopy of quadrupolar nuclei
    • C. Jäger Satellite transition spectroscopy of quadrupolar nuclei NMR Basic Principles Prog. 31 1994 133 170
    • (1994) NMR Basic Principles Prog. , vol.31 , pp. 133-170
    • Jäger, C.1
  • 27
    • 0035366873 scopus 로고    scopus 로고
    • Measurement of molecular motion in solids by nuclear magnetic resonance spectroscopy of half-integer quadrupole nuclei
    • J.H. Kristensen, and I. Farnan Measurement of molecular motion in solids by nuclear magnetic resonance spectroscopy of half-integer quadrupole nuclei J. Chem. Phys. 114 21 2001 9608 9624
    • (2001) J. Chem. Phys. , vol.114 , Issue.21 , pp. 9608-9624
    • Kristensen, J.H.1    Farnan, I.2
  • 28
    • 0030195939 scopus 로고    scopus 로고
    • Redetermination of l-leucine at 120 K
    • C.H. Gorbitz, and B. Dalhus Redetermination of l-leucine at 120 K Acta Crystallogr. C 52 1996 1754 1756
    • (1996) Acta Crystallogr. C , vol.52 , pp. 1754-1756
    • Gorbitz, C.H.1    Dalhus, B.2
  • 29
    • 0015515825 scopus 로고
    • Precision neutron diffraction structure determination of protein and nucleic acid components, I: The crystal and molecular structure of the amino acid l-alanine
    • M.S. Lehmann, T.F. Koetzle, and W.C. Hamilton Precision neutron diffraction structure determination of protein and nucleic acid components, I: the crystal and molecular structure of the amino acid l-alanine J. Am. Chem. Soc. 94 8 1971 2657 2660
    • (1971) J. Am. Chem. Soc. , vol.94 , Issue.8 , pp. 2657-2660
    • Lehmann, M.S.1    Koetzle, T.F.2    Hamilton, W.C.3
  • 30
    • 0043194331 scopus 로고    scopus 로고
    • Interatomic distance measurement in solid-state NMR between a spin-(1)/(2) and a spin-(5)/(2) using a universal REAPDOR curve
    • A. Goldbourt, S. Vega, T. Gullion, and A.J. Vega Interatomic distance measurement in solid-state NMR between a spin-(1)/(2) and a spin-(5)/(2) using a universal REAPDOR curve J. Am. Chem. Soc. 125 37 2003 11194 11195
    • (2003) J. Am. Chem. Soc. , vol.125 , Issue.37 , pp. 11194-11195
    • Goldbourt, A.1    Vega, S.2    Gullion, T.3    Vega, A.J.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.